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HomeProduct name listTRIMETHYLSILYLMETHYL AZIDE

TRIMETHYLSILYLMETHYL AZIDE

TRIMETHYLSILYLMETHYL AZIDE Structural

What is TRIMETHYLSILYLMETHYL AZIDE?

Physical properties

bp 43 °C/43 mmHg; IR νmax 2100 cm?1; 1H NMR (CDCl3) δ = 0.12 (s, 9H), 2.75 (s, 2H); MS m/z 129, 73.

The Uses of TRIMETHYLSILYLMETHYL AZIDE

Trimethylsilylmethyl Azide is used in the amination of organometallic compounds; preparation of heterocyclic compounds; precursor of azomethine ylide, reactant in Silylmethyl-Substituted Heterocumulenes and [3 + 2] Cycloaddition etc.

Preparation

Obtained in high yield by reaction of sodium azide and (chloromethyl)trimethylsilane in DMF or HMPA at 80°C.

Properties of TRIMETHYLSILYLMETHYL AZIDE

Boiling point: 92-95°C
Density  0,87 g/cm3
refractive index  1.4300 to 1.4340
Flash point: 6°C
solubility  Sol organic solvents; insol water.
form  clear liquid
Specific Gravity 0.87
color  Colorless to Yellow to Green
Hydrolytic Sensitivity 7: reacts slowly with moisture/water

Safety information for TRIMETHYLSILYLMETHYL AZIDE

Computed Descriptors for TRIMETHYLSILYLMETHYL AZIDE

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