Contact us: +91 9550333722 040 - 40102781
Structured search
India
Choose your country
Different countries will display different contents
Try our best to find the right business for you.
My chemicalbook

Welcome back!

HomeProduct name listN,N-Dibenzylhydroxylamine

N,N-Dibenzylhydroxylamine

  • CAS NO.:621-07-8
  • Empirical Formula: C14H15NO
  • Molecular Weight: 213.27
  • MDL number: MFCD00004772
  • EINECS: 210-667-1
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-11-04 20:04:50
N,N-Dibenzylhydroxylamine Structural

What is N,N-Dibenzylhydroxylamine?

Chemical properties

white to slightly yellow adhering crystalline

The Uses of N,N-Dibenzylhydroxylamine

N,N-Dibenzylhydroxylamine, upon oxidation, yields N-benzyl-α-phenylnitrone, which can undergo cycloaddition reaction with suitable dipolarophiles. It can be used to synthesize N,N,O-trisubstituted hydroxylamines and arylamines.

Preparation

A mixture of 14 gm (0.202 mole) of hydroxylamine hydrochloride and 50 gm (0.395 mole) of benzyl chloride in 200 ml of 70% ethanol is treated with 60 gm of crystalline sodium carbonate. The mixture is heated under a reflux condenser for 2 hr, cooled to room temperature, filtered, and the solids discarded. The filtrate is treated with sufficient ice water to cause precipitation of A^N-dibenzylhydroxylamine. The reaction mixture is then thoroughly cooled in a freezing mixture to permit complete precipitation of product to take place. The yield, upon filtration, is 26 gm (61.5%), m.p. 123°C. A similar preparation has recently been reported [13a].
621-07-8 synthesis

Properties of N,N-Dibenzylhydroxylamine

Melting point: 125-128 °C (lit.)
Boiling point: 353.27°C (rough estimate)
Density  1.0439 (rough estimate)
refractive index  1.5300 (estimate)
storage temp.  Inert atmosphere,Store in freezer, under -20°C
Water Solubility  Insoluble in water
form  powder to crystal
pka 13.19±0.69(Predicted)
color  White to Almost white
BRN  978234
CAS DataBase Reference 621-07-8(CAS DataBase Reference)
NIST Chemistry Reference Hydroxylamine, n,n-dibenzyl-,(621-07-8)
EPA Substance Registry System Benzenemethanamine, N-hydroxy-N-(phenylmethyl)- (621-07-8)

Safety information for N,N-Dibenzylhydroxylamine

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P261:Avoid breathing dust/fume/gas/mist/vapours/spray.
P264:Wash hands thoroughly after handling.
P264:Wash skin thouroughly after handling.
P271:Use only outdoors or in a well-ventilated area.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352:IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for N,N-Dibenzylhydroxylamine

Related products of tetrahydrofuran

You may like

  • 621-07-8 Dibenzyl hydroxylamine 99%
    621-07-8 Dibenzyl hydroxylamine 99%
    621-07-8
    View Details
  • N,N-Dibenzylhydroxylamine 95% CAS 621-07-8
    N,N-Dibenzylhydroxylamine 95% CAS 621-07-8
    621-07-8
    View Details
  • N,N-Dibenzylhydroxylamine CAS 621-07-8
    N,N-Dibenzylhydroxylamine CAS 621-07-8
    621-07-8
    View Details
  • N,N-Dibenzylhydroxylamine CAS 621-07-8
    N,N-Dibenzylhydroxylamine CAS 621-07-8
    621-07-8
    View Details
  • 1823368-42-8 98%
    1823368-42-8 98%
    1823368-42-8
    View Details
  • 2-(3-(tert-butyl)phenoxy)-2-methylpropanoic acid 1307449-08-6 98%
    2-(3-(tert-butyl)phenoxy)-2-methylpropanoic acid 1307449-08-6 98%
    1307449-08-6
    View Details
  • Ethyl 3-(furan-2-yl)-3-hydroxypropanoate 25408-95-1 98%
    Ethyl 3-(furan-2-yl)-3-hydroxypropanoate 25408-95-1 98%
    25408-95-1
    View Details
  • Lithium Clavulanate
    Lithium Clavulanate
    61177-44-4
    View Details
Statement: All products displayed on this website are only used for non medical purposes such as industrial applications or scientific research, and cannot be used for clinical diagnosis or treatment of humans or animals. They are not medicinal or edible.