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HomeProduct name listEthyl 3-(pyridin-2-ylamino)propanoate

Ethyl 3-(pyridin-2-ylamino)propanoate

  • CAS NO.:103041-38-9
  • Empirical Formula: C10H14N2O2
  • Molecular Weight: 194.23
  • MDL number: MFCD09833621
  • EINECS: 600-382-4
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-08-21 22:41:43
Ethyl 3-(pyridin-2-ylamino)propanoate Structural

What is Ethyl 3-(pyridin-2-ylamino)propanoate?

Chemical properties

White Solid

The Uses of Ethyl 3-(pyridin-2-ylamino)propanoate

Ethyl 3-(2-Pyridylamino)propanoate is an intermediate used in the synthesis of Dabigatran etexilate, as thrombin inhibitors. Ethyl Ester form of P993315.

Synthesis

A method for preparing Ethyl 3-(pyridin-2-ylamino)propanoate comprises the following steps: using 2-aminopyridine and ethyl acrylate as raw materials, using anhydrous ethanol as a solvent, using trifluoromethanesulfonic acid as a catalyst, and heating in an oil bath to control the temperature at 120 to 160° C. for a catalytic reaction for 16 to 20 hours under nitrogen protection. The obtained reaction solution is washed with petroleum ether at a temperature of 35 to 40° C. and a pressure of 0.09 to 0.1 MPa, then concentrated under reduced pressure, and then washed with petroleum ether/ethyl acetate and recrystallized to obtain white flaky crystals of Ethyl 3-(pyridin-2-ylamino)propanoate.

Properties of Ethyl 3-(pyridin-2-ylamino)propanoate

Melting point: 48-50°C
Boiling point: 125°C/0.2mmHg(lit.)
Density  1.131±0.06 g/cm3(Predicted)
storage temp.  Keep in dark place,Inert atmosphere,2-8°C
solubility  DMSO, Methanol
form  Solid
pka 6.26±0.10(Predicted)
color  White
InChI InChI=1S/C10H14N2O2/c1-2-14-10(13)6-8-12-9-5-3-4-7-11-9/h3-5,7H,2,6,8H2,1H3,(H,11,12)

Safety information for Ethyl 3-(pyridin-2-ylamino)propanoate

Computed Descriptors for Ethyl 3-(pyridin-2-ylamino)propanoate

InChIKey UITNIDFEANEWPC-UHFFFAOYSA-N
SMILES C(OCC)(=O)CCNC1C=CC=CN=1

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