Ethyltriphenylphosphonium iodide
Synonym(s):ETPPI;Phenylphosphonium ethyl iodide
- CAS NO.:4736-60-1
- Empirical Formula: C20H20IP
- Molecular Weight: 418.251031
- MDL number: MFCD00040352
- EINECS: 225-245-2
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-08-12 17:17:06
What is Ethyltriphenylphosphonium iodide?
Chemical properties
Ethyltriphenylphosphonium iodide is white to slightly yellowish crystalline powder
The Uses of Ethyltriphenylphosphonium iodide
Ethyltriphenylphosphonium iodide is used as a Wittig reagent and phase transfer catalyst in organic synthesis. It can also be used in asymmetric hydrogenation and to make Bismuth(III) polynuclear complexes.
The Uses of Ethyltriphenylphosphonium iodide
Ethyltriphenylphosphonium iodide is involved in synthesis of diarylmethine derivatives, phosphonium salts, and bismuth(III) polynuclear halide complexes, asymmetric hydrogenation.
Flammability and Explosibility
Not classified
Synthesis
(1) adding triphenyl phosphine to an organic solvent, adding ethyl chloride in a dropwise manner, heating to a temperature of 120-160℃ after the adding, adjusting the reaction pressure to 8-12 kg/cm2, and carrying out a thermal insulation reaction for 30-40 h; (2) after completing the thermal insulation reaction, cooling to a room temperature, reducing the pressure to a normal pressure, and carrying out centrifugation on the material obtained after the reaction; and (3) drying the centrifugal precipitate so as to obtain the ethyl triphenyl phosphonium chloride.
Properties of Ethyltriphenylphosphonium iodide
Melting point: | 164-168 °C(lit.) |
Boiling point: | 337 °C |
Density | 1.500 |
vapor pressure | 0Pa at 25℃ |
Flash point: | 226 °C |
storage temp. | Keep in dark place,Inert atmosphere,Room temperature |
solubility | Acetone, Chloroform, Dichloromethane, Methanol |
form | Powder |
color | Yellow |
Water Solubility | slightly soluble |
Sensitive | Light Sensitive & Hygroscopic |
BRN | 3659323 |
CAS DataBase Reference | 4736-60-1(CAS DataBase Reference) |
EPA Substance Registry System | Phosphonium, ethyltriphenyl-, iodide (4736-60-1) |
Safety information for Ethyltriphenylphosphonium iodide
Signal word | Danger |
Pictogram(s) |
Skull and Crossbones Acute Toxicity GHS06 |
GHS Hazard Statements |
H301:Acute toxicity,oral H319:Serious eye damage/eye irritation |
Precautionary Statement Codes |
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for Ethyltriphenylphosphonium iodide
InChIKey | SLAFUPJSGFVWPP-UHFFFAOYSA-M |
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