CYCLODECANONE

CAS NO.：1502-06-3
Empirical Formula: C10H18O
Molecular Weight: 154.25
MDL number: MFCD00003713
EINECS: 216-119-8
SAFETY DATA SHEET (SDS)
Update Date: 2023-05-25 18:01:14

What is CYCLODECANONE?

Chemical properties

White solid or colorless liquid

Synthesis Reference(s)

Journal of the American Chemical Society, 86, p. 3068, 1964 DOI: 10.1021/ja01069a019
Organic Syntheses, Coll. Vol. 4, p. 218, 1963
Synthetic Communications, 9, p. 437, 1979 DOI: 10.1080/00397917908064174

Purification Methods

Purify the ketone via the semicarbazone (m 205-207o, from EtOH) and distil it through an efficient column. It sublimes in a vacuum. The oxime has m 80o, from MeOH or by sublimation in a high vacuum. [Cope et al. Org Synth Coll Vol IV 218 1963, Prelog et al. Helv Chim Acta 30 1746 1947, Ruzicka et al. Helv Chim Acta 11 675 1930, Beilstein 7 III 134, 7 IV 76.]

Properties of CYCLODECANONE

Melting point:	21-24 °C (lit.)
Boiling point:	106-107 °C/12 mmHg (lit.)
Density	0.958 g/mL at 25 °C (lit.)
refractive index	n20/D 1.482(lit.)
Flash point:	180 °F
storage temp.	2-8°C
solubility	Chloroform (Slightly), Methanol (Slightly)
form	Colourless Oil to Semi-Solid
BRN	1617127

Safety information for CYCLODECANONE

Signal word	Warning
Pictogram(s)	Exclamation Mark Irritant GHS07
GHS Hazard Statements	H319:Serious eye damage/eye irritation
Precautionary Statement Codes	P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.