5,6,7,7a-Tetrahydrothieno[3,2-c]pyridine-2(4H)-one hydrochloride
- CAS NO.:115473-15-9
- Empirical Formula: C7H10ClNOS
- Molecular Weight: 191.67
- MDL number: MFCD11111130
- EINECS: 601-365-4
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-10-29 11:48:30
What is 5,6,7,7a-Tetrahydrothieno[3,2-c]pyridine-2(4H)-one hydrochloride?
Chemical properties
Cream Solid
The Uses of 5,6,7,7a-Tetrahydrothieno[3,2-c]pyridine-2(4H)-one hydrochloride
Solifenacin intermediate
The Uses of 5,6,7,7a-Tetrahydrothieno[3,2-c]pyridine-2(4H)-one hydrochloride
5,6,7,7a-tetrahydrothieno[3,2-c]pyridin-2(4H)-one hydrochloride is used as an intermediate in the synthesis of Prasugrel (P701150).
Synthesis
Hydrochloride (0.32 ml) was added in a solution of 5-Triphenyl methyl-tetrahydro-5, 6, 7,7a 4H- theino-[3,2-c]- pyridone-2 (100 g, 0.25 moles) in acetone (500 ml) at 25 °C. Stir the reaction mass for 1 hr at 50 °C, then cool the reaction mass to 25 °C and stir for 8 to 10 hrs at 25 °C. Filter the product and wash it with acetone. Dry the material under vacuum at 60 °C to obtain 5, 6, 7,7a -Tetrahydro-4H- theino-[3,2-c]- pyridone-2 hydrochloride (42 g, 99percent).
Properties of 5,6,7,7a-Tetrahydrothieno[3,2-c]pyridine-2(4H)-one hydrochloride
Melting point: | 2100C (dec) |
storage temp. | Inert atmosphere,Store in freezer, under -20°C |
solubility | DMSO, Methanol, Water |
form | Solid |
color | Light Tan |
InChI | InChI=1S/C7H9NOS.ClH/c9-7-3-5-4-8-2-1-6(5)10-7;/h3,6,8H,1-2,4H2;1H |
CAS DataBase Reference | 115473-15-9(CAS DataBase Reference) |
Safety information for 5,6,7,7a-Tetrahydrothieno[3,2-c]pyridine-2(4H)-one hydrochloride
Signal word | Warning |
Pictogram(s) |
Exclamation Mark Irritant GHS07 |
GHS Hazard Statements |
H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation |
Precautionary Statement Codes |
P280:Wear protective gloves/protective clothing/eye protection/face protection. P302+P352:IF ON SKIN: wash with plenty of soap and water. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. P332+P313:IF SKIN irritation occurs: Get medical advice/attention. P337+P313:IF eye irritation persists: Get medical advice/attention. |
Computed Descriptors for 5,6,7,7a-Tetrahydrothieno[3,2-c]pyridine-2(4H)-one hydrochloride
InChIKey | PUQKTVAKLPDUAW-UHFFFAOYSA-N |
SMILES | O=C1SC2CCNCC2=C1.Cl |
Abamectin manufacturer
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