4,4'-Oxybis(benzoyl Chloride)
- CAS NO.:7158-32-9
- Empirical Formula: C14H8Cl2O3
- Molecular Weight: 295.12
- MDL number: MFCD00496619
- EINECS: 808-159-5
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-10-28 23:16:16
What is 4,4'-Oxybis(benzoyl Chloride)?
The Uses of 4,4'-Oxybis(benzoyl Chloride)
4,4'-OXYBISBENZOYL CHLORIDE is a useful research chemical.
The Uses of 4,4'-Oxybis(benzoyl Chloride)
4,4'-Oxybis(benzoyl Chloride) is a monomer used in high-performance polymers for the preparation of a new low-temperature curing photosensitive polymer (PHA-6F). The polymer exhibits high transparency at 365 nm (i-line). The photosensitivity and contrast of the 2.4 μm thick film were 15 mJ/cm2 and 2.5, respectively.
Synthesis
4,4′-oxybisbenzaldehyde is reacted with chlorine to produce 4,4'-Oxybis(benzoyl Chloride) in high yield without using a large amount of reaction solvent. A 300 ml four-necked flask equipped with a stirrer, a thermometer and a reflux condenser was charged with 90.6 g (0.40 mol) of 4,4′-oxybisbenzaldehyde and 158.6 g of PCBTF, and heated and stirred to 143 ° C. The temperature was raised to. A high pressure mercury lamp was turned on and irradiated with light. The reaction was started by supplying chlorine gas at a chlorine gas blowing rate of 0.06 mol / hour so as to maintain a reaction temperature of 143 ° C. (reflux). After 15 hours from the start of the reaction, disappearance of the raw materials was confirmed by gas chromatography, and the reaction was completed. When this was analyzed using gas chromatography, the reaction yield of 4,4'-Oxybis(benzoyl Chloride) was 98.6% by mass.
Properties of 4,4'-Oxybis(benzoyl Chloride)
Melting point: | 22-23℃ |
Boiling point: | 404℃ |
Density | 1.386 |
Flash point: | 164℃ |
storage temp. | under inert gas (nitrogen or Argon) at 2-8°C |
solubility | soluble in Toluene |
form | powder to crystaline |
color | White to Almost white |
InChI | InChI=1S/C14H8Cl2O3/c15-13(17)9-1-5-11(6-2-9)19-12-7-3-10(4-8-12)14(16)18/h1-8H |
Safety information for 4,4'-Oxybis(benzoyl Chloride)
Signal word | Danger |
Pictogram(s) |
Corrosion Corrosives GHS05 Exclamation Mark Irritant GHS07 |
GHS Hazard Statements |
H302:Acute toxicity,oral H312:Acute toxicity,dermal H314:Skin corrosion/irritation H332:Acute toxicity,inhalation |
Precautionary Statement Codes |
P260:Do not breathe dust/fume/gas/mist/vapours/spray. P261:Avoid breathing dust/fume/gas/mist/vapours/spray. P264:Wash hands thoroughly after handling. P264:Wash skin thouroughly after handling. P270:Do not eat, drink or smoke when using this product. P271:Use only outdoors or in a well-ventilated area. P280:Wear protective gloves/protective clothing/eye protection/face protection. P310:Immediately call a POISON CENTER or doctor/physician. P312:Call a POISON CENTER or doctor/physician if you feel unwell. P321:Specific treatment (see … on this label). P322:Specific measures (see …on this label). P330:Rinse mouth. P363:Wash contaminated clothing before reuse. P301+P312:IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell. P301+P330+P331:IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P302+P352:IF ON SKIN: wash with plenty of soap and water. P303+P361+P353:IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower. P304+P340:IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. P405:Store locked up. P501:Dispose of contents/container to..… |
Computed Descriptors for 4,4'-Oxybis(benzoyl Chloride)
InChIKey | OSUWBBMPVXVSOA-UHFFFAOYSA-N |
SMILES | O(C1=CC=C(C=C1)C(Cl)=O)C1=CC=C(C=C1)C(Cl)=O |
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