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HomeProduct name list3-Nitropyridine

3-Nitropyridine

3-Nitropyridine Structural

What is 3-Nitropyridine?

Chemical properties

white to yellow needle-like crystals

The Uses of 3-Nitropyridine

3-Nitropyridine is used in the novel synthesis of biologically active nitro heterocyclic compounds.

Synthesis

In 1993 Suzuki and co-workers reported the nitration of pyridine with nitrogen dioxide and ozone in dichloromethane at room temperature. They obtained a 3.5 % yield of 3-nitropyridine and 1.2 % of 3,5-dinitropyridine.
3-Nitropyridine synthesis from nitration of pyridine
3-Nitropyridines can also be synthesized by oxidation of 3-aminopyridine with hydrogen peroxide in fuming sulphuric acid in 45% yield. Nitration of 2,6-dichloropyridine with nitronium tetrafluoroborate gave a 11% yield of 3-nitropyridine after dehalogenation. 3-nitropyridine has also been prepared from 2- chloro-3-nitropyridine.

Properties of 3-Nitropyridine

Melting point: 35-40 °C
Boiling point: 216°C
Density  1,33 g/cm3
refractive index  1.4800 (estimate)
Flash point: 216°C
storage temp.  Flammables area
solubility  soluble in Methanol
pka pK1:0.79(+1) (25°C,μ=0.02)
form  Liquid
color  Clear colorless
BRN  111969
CAS DataBase Reference 2530-26-9(CAS DataBase Reference)

Safety information for 3-Nitropyridine

Signal word Danger
Pictogram(s)
ghs
Corrosion
Corrosives
GHS05
ghs
Skull and Crossbones
Acute Toxicity
GHS06
GHS Hazard Statements H301:Acute toxicity,oral
H315:Skin corrosion/irritation
H318:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P280:Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352:IF ON SKIN: wash with plenty of soap and water.

Computed Descriptors for 3-Nitropyridine

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