(-)-Isopinocampheol
Synonym(s):(−)-Isopinocampheol;(1R,2R,3R,5S)-2,6,6-Trimethylbicyclo[3.1.1]heptan-3-ol;(1R,2R,3R,5S)-3-Pinanol;3-Pinanol
- CAS NO.：25465-65-0
- Empirical Formula: C10H18O
- Molecular Weight: 154.25
- MDL number: MFCD00064146
- EINECS: 247-011-9
- SAFETY DATA SHEET (SDS)
- Update Date: 2023-05-25 18:01:00
What is (-)-Isopinocampheol?
Purification Methods
Dissolve it in Et2O, dry over MgSO4, filter, evaporate, then recrystallise it from pet ether. Also recrystallise it from aqueous EtOH and distil it in a vacuum. [Kergomard & Geneix Bull Soc Chim Fr 394 1958, Zweifel & Brown J Am Chem Soc 86 393 1964.] The 3,4-dinitrobenzoyl derivative has m 100-101o, the phenylcarbamoyl derivative has m 137-138o and the acid -phthalate has m 125-126o. [Beilstein 6 III 282, 283.]
Properties of (-)-Isopinocampheol
| Melting point: | 52-55 °C |
| Boiling point: | 219 °C(lit.) |
| alpha | -34 º (c=20, EtOH) |
| Density | 0.8389 (rough estimate) |
| refractive index | 1.4710 (estimate) |
| Flash point: | 200 °F |
| pka | 15.35±0.60(Predicted) |
| optical activity | [α]22/D 34°, c = 20 in ethanol |
| BRN | 2038100 |
Safety information for (-)-Isopinocampheol
Computed Descriptors for (-)-Isopinocampheol
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