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HomeProduct name listN,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

Synonym(s):Ishikawa’s Reagent

  • CAS NO.:309-88-6
  • Empirical Formula: C7H11F6N
  • Molecular Weight: 223.16
  • MDL number: MFCD00054683
  • EINECS: 628-698-8
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2023-04-23 13:52:06
N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine Structural

What is N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine?

Chemical properties

Clear colorless to yellow liquid

The Uses of N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

Demonstrates utility in fluorination.7

The Uses of N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

Fluorinating agent.

The Uses of N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

Reactant for:

  • Friedel-Crafts type arylation of hydrofluorocarbons
  • Microbial hydroxylation of antibiotics
  • Electrochemical fluorination of trialkylamines and tetraalkylammonium salts
  • Fluorination of pyrethroides

Reactant for synthesis of:
  • γ-Hydroxy-α-fluoro-α-trifluoromethylcarboxamide
  • Florfenicol and thiamphenicol

What are the applications of Application

Ishikawa′s Reagent is An inserter of fluoro(trifluoromethyl) methylene moiety in unsaturated alcohols

General Description

GC analysis includes Et2NCF=CFCF3 (two isomers), both of which are active fluorinating agents.

Properties of N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

Boiling point: 56-57 °C (lit.)
Density  1.230 g/mL at 25 °C (lit.)
refractive index  1.3460
Flash point: 56-57°C/58mm
storage temp.  Flammables area
solubility  soluble in Acetone,Ether
form  Liquid
pka 1.50±0.70(Predicted)
Specific Gravity 1.230
color  Clear colorless to yellow
Merck  14,5108
CAS DataBase Reference 309-88-6(CAS DataBase Reference)
EPA Substance Registry System N,N-Diethyl-2H-perfluoropropanamine (309-88-6)

Safety information for N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

Signal word Danger
Pictogram(s)
ghs
Flame
Flammables
GHS02
ghs
Corrosion
Corrosives
GHS05
GHS Hazard Statements H226:Flammable liquids
H314:Skin corrosion/irritation
Precautionary Statement Codes P210:Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P233:Keep container tightly closed.
P240:Ground/bond container and receiving equipment.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353:IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for N,N-Diethyl-1,1,2,3,3,3-hexafluoropropylamine

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