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HomeProduct name listN-Methyl-N-nitrosotoluene-4-sulphonamide

N-Methyl-N-nitrosotoluene-4-sulphonamide

Synonym(s):N-Methyl-N-nitroso-p-toluenesulfonamide

  • CAS NO.:80-11-5
  • Empirical Formula: C8H10N2O3S
  • Molecular Weight: 214.24
  • MDL number: MFCD00002050
  • EINECS: 201-252-6
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-12-18 14:08:57
N-Methyl-N-nitrosotoluene-4-sulphonamide Structural

What is N-Methyl-N-nitrosotoluene-4-sulphonamide?

Chemical properties

pale yellow crystalline powder

The Uses of N-Methyl-N-nitrosotoluene-4-sulphonamide

N-Methyl-N-nitroso-p-toluenesulfonamide is Diazomethane precursor.

The Uses of N-Methyl-N-nitrosotoluene-4-sulphonamide

In the laboratory preparation of diazomethane. Directions for use: de Boer, Backer, Rec. Trav. Chim. 73, 232 (1954).

Definition

ChEBI: N,4-dimethyl-N-nitrosobenzenesulfonamide is a sulfonamide.

Purification Methods

Crystallise diazald from *benzene by addition of pet ether and store it in a refrigerator. It is soluble in most organic solvents and liberates diazomethane on treatment with alkali. Store it in the cold. [deBoer & Backer Org Synth 34 96 1954, Beilstein 11 I 29.]

Properties of N-Methyl-N-nitrosotoluene-4-sulphonamide

Melting point: ~58 °C
Boiling point: 320.5±35.0 °C(Predicted)
Density  1.3844 (rough estimate)
refractive index  1.5690 (estimate)
storage temp.  2-8°C
solubility  Chloroform (Slightly), Dichloromethane (Sparingly), DMSO (Slightly), Ethyl Acetate
pka -19.25±0.70(Predicted)
form  Solid
color  Pale Yellow to Yellow
Merck  13,9621
Stability: Stable, but heat sensitive; may also be light sensitive. Incompatible with strong oxidizing agents, alkalies.
CAS DataBase Reference 80-11-5(CAS DataBase Reference)
NIST Chemistry Reference N-methyl-n-nitroso, p-toluene sulfonamide(80-11-5)
EPA Substance Registry System Benzenesulfonamide, N,4-dimethyl-N-nitroso- (80-11-5)

Safety information for N-Methyl-N-nitrosotoluene-4-sulphonamide

Computed Descriptors for N-Methyl-N-nitrosotoluene-4-sulphonamide

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