N-Methyl-N-nitrosotoluene-4-sulphonamide
Synonym(s):N-Methyl-N-nitroso-p-toluenesulfonamide
- CAS NO.：80-11-5
- Empirical Formula: C8H10N2O3S
- Molecular Weight: 214.24
- MDL number: MFCD00002050
- EINECS: 201-252-6
- SAFETY DATA SHEET (SDS)
- Update Date: 2023-05-15 10:44:00
What is N-Methyl-N-nitrosotoluene-4-sulphonamide?
Chemical properties
pale yellow crystalline powder
The Uses of N-Methyl-N-nitrosotoluene-4-sulphonamide
N-Methyl-N-nitroso-p-toluenesulfonamide is Diazomethane precursor.
The Uses of N-Methyl-N-nitrosotoluene-4-sulphonamide
In the laboratory preparation of diazomethane. Directions for use: de Boer, Backer, Rec. Trav. Chim. 73, 232 (1954).
Definition
ChEBI: N,4-dimethyl-N-nitrosobenzenesulfonamide is a sulfonamide.
Purification Methods
Crystallise diazald from *benzene by addition of pet ether and store it in a refrigerator. It is soluble in most organic solvents and liberates diazomethane on treatment with alkali. Store it in the cold. [deBoer & Backer Org Synth 34 96 1954, Beilstein 11 I 29.]
Properties of N-Methyl-N-nitrosotoluene-4-sulphonamide
| Melting point: | ~58 °C |
| Boiling point: | 320.5±35.0 °C(Predicted) |
| Density | 1.3844 (rough estimate) |
| refractive index | 1.5690 (estimate) |
| storage temp. | 2-8°C |
| solubility | Chloroform (Slightly), Dichloromethane (Sparingly), DMSO (Slightly), Ethyl Acetate |
| pka | -19.25±0.70(Predicted) |
| form | Solid |
| color | Pale Yellow to Yellow |
| Merck | 13,9621 |
| Stability: | Stable, but heat sensitive; may also be light sensitive. Incompatible with strong oxidizing agents, alkalies. |
| CAS DataBase Reference | 80-11-5(CAS DataBase Reference) |
| NIST Chemistry Reference | N-methyl-n-nitroso, p-toluene sulfonamide(80-11-5) |
| EPA Substance Registry System | Benzenesulfonamide, N,4-dimethyl-N-nitroso- (80-11-5) |
Safety information for N-Methyl-N-nitrosotoluene-4-sulphonamide
Computed Descriptors for N-Methyl-N-nitrosotoluene-4-sulphonamide
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