Ethyl N-cyanoethanimideate
- CAS NO.：1558-82-3
- Empirical Formula: C5H8N2O
- Molecular Weight: 112.13
- MDL number: MFCD03411888
- SAFETY DATA SHEET (SDS)
- Update Date: 2023-06-08 17:06:38
What is Ethyl N-cyanoethanimideate?
Preparation
To a flask equipped as in Preparation 2-6 is added 162.0 gm (1.0 mole) of ethyl orthoacetate, 42.0 gm (1.0 mole) of cyanamide, and 134.0 gm (2.0 moles) of acetic anhydride. The reaction mixture is heated to 130-140°C and the ethyl acetate and acetic acid are distilled over. The heat is removed until the initial vigorous reaction subsides and then the heating is continued at 135-140°C until most of the remaining ethyl acetate and acetid acid have distilled over (approx. 1 hr). The residue is then distilled under reduced pressure to afford 100.8 gm (90%), b.p. 90-95°C (20 mm Hg).
Properties of Ethyl N-cyanoethanimideate
| Melting point: | 78-81 °C(Solv: ethyl ether (60-29-7)) |
| Boiling point: | 133.2±23.0 °C(Predicted) |
| Density | 0.94 |
| refractive index | 1.45 |
| storage temp. | 2-8°C |
| pka | -2.94±0.50(Predicted) |
| CAS DataBase Reference | 1558-82-3(CAS DataBase Reference) |
Safety information for Ethyl N-cyanoethanimideate
Computed Descriptors for Ethyl N-cyanoethanimideate
Ethyl N-cyanoethanimideate manufacturer
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