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HomeProduct name listCIS-3,4-DICHLOROCYCLOBUTENE

CIS-3,4-DICHLOROCYCLOBUTENE

CIS-3,4-DICHLOROCYCLOBUTENE Structural

What is CIS-3,4-DICHLOROCYCLOBUTENE?

Purification Methods

Distil the cyclobutene at 55mm through a 36-in platinum spinning band column, a fore-run b 58-62o/55mm is mainly 1,4-dichlorobutadiene. When the temperature reaches 70o the reflux ratio is reduced to 10:1 and the product is collected quickly. It is usually necessary to apply heat frequently with a sun lamp to prevent any dichlorobutadiene from clogging the exit in the early part of the distillation [Pettit & Henery Org Synth 50 36 1970].

Properties of CIS-3,4-DICHLOROCYCLOBUTENE

Boiling point: 74-76 °C55 mm Hg(lit.)
Density  1.302 g/mL at 20 °C(lit.)
refractive index  n20/D 1.503
Flash point: 55 °C
storage temp.  2-8°C

Safety information for CIS-3,4-DICHLOROCYCLOBUTENE

Signal word Warning
Pictogram(s)
ghs
Flame
Flammables
GHS02
GHS Hazard Statements H226:Flammable liquids

Computed Descriptors for CIS-3,4-DICHLOROCYCLOBUTENE

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