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HomeProduct name list3-Picoline-N-oxide

3-Picoline-N-oxide

Synonym(s):3-Methylpyridine 1-oxide;3-Picoline N-oxide

  • CAS NO.:1003-73-2
  • Empirical Formula: C6H7NO
  • Molecular Weight: 109.13
  • MDL number: MFCD00006203
  • EINECS: 213-714-4
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-07-25 20:04:51
3-Picoline-N-oxide Structural

What is 3-Picoline-N-oxide?

Chemical properties

PALE YELLOW TO BROWN CRYSTALLINE LOW MELTING MASS

The Uses of 3-Picoline-N-oxide

An intermediate in the preparation of nicotine derivatives.

Purification Methods

Purify the N-oxide by careful fractionation in vacuo. The distillate remains supercooled for several days before solidifying. It is a slightly hygroscopic solid which could melt in the hand. The picrate has m 149-151o (from EtOH). [Taylor & Corvetti Org Synth Coll Vol IV 654 1963, IR: Katritzky et al. J Chem Soc 3680 1959, Jaffé & Doak J Am Chem Soc 77 4441, 4481 1955, Boekelheide & Linn J Am Chem Soc 76 1286 1954]. [Beilstein 20 III/IV 2719, 20/5 V 517.]

Properties of 3-Picoline-N-oxide

Melting point: 37-39 °C(lit.)
Boiling point: 150 °C15 mm Hg(lit.)
Density  1.13
refractive index  1.5444 (estimate)
Flash point: >230 °F
storage temp.  Sealed in dry,Room Temperature
solubility  >2000g/l
pka pK1:10.921(+1) (25°C)
form  Crystalline Low Melting Mass
color  Pale yellow to brown
Water Solubility  soluble
Sensitive  Hygroscopic
BRN  106327
CAS DataBase Reference 1003-73-2(CAS DataBase Reference)
NIST Chemistry Reference Pyridine, 3-methyl-, 1-oxide(1003-73-2)
EPA Substance Registry System Pyridine, 3-methyl-, 1-oxide (1003-73-2)

Safety information for 3-Picoline-N-oxide

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
Precautionary Statement Codes P264:Wash hands thoroughly after handling.
P264:Wash skin thouroughly after handling.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352:IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313:IF SKIN irritation occurs: Get medical advice/attention.
P337+P313:IF eye irritation persists: Get medical advice/attention.

Computed Descriptors for 3-Picoline-N-oxide

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