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HomeProduct name list2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride

2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride

Synonym(s):2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride;Dimethyl[(2-oxocyclohexyl)methyl]ammonium chloride

2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride Structural

What is 2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride?

Chemical properties

white crystalline powder

The Uses of 2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride

An impurity found in Tramadol (T712500).

Synthesis

0.982 g (1.03 mL, 10.0 mmol) cyclohexanone, 0.360 g (12.0 mmol) paraformaldehyde, 0.816 g (10.0 mmol) dimethylammonium chloride and 4 mL ethanol are filled in a 25 mL round bottom flask with reflux condenser and magnetic stir bar. 2 drops of conc. hydrochloric acid is added, and the mixture is heated under stirring for 4 hours under reflux. The hot solution is filtered in a round bottom flask, and the solvent is evaporated by the rotary evaporator. The residue is dissolved in 2 mL ethanol under heating. At room temperature, 20 mL acetone is added to the solution. For complete crystallization, the solution is stored overnight in the freezer compartment. The crystallized crude product 2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride is sucked off over a Buechner funnel and dried in the desiccator over silica gel.
2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride

Properties of 2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride

Melting point: 147-151 °C
storage temp.  2-8°C
solubility  Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
form  Crystalline Powder
color  White
Water Solubility  soluble
InChI InChI=1S/C9H17NO.ClH/c1-10(2)7-8-5-3-4-6-9(8)11;/h8H,3-7H2,1-2H3;1H
CAS DataBase Reference 42036-65-7(CAS DataBase Reference)

Safety information for 2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride

Signal word Danger
Pictogram(s)
ghs
Corrosion
Corrosives
GHS05
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H318:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P280:Wear protective gloves/protective clothing/eye protection/face protection.

Computed Descriptors for 2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride

InChIKey CLVHTSWMNNSUSH-UHFFFAOYSA-N
SMILES C1(CN(C)C)CCCCC1=O.Cl

Abamectin manufacturer

GLP Pharma Standards

2Y
Phone:+91-9866074638
Whatsapp: +91 9866074638
product: Tramadol EP Impurity-E 98%
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KARPSCHEM LABORATORIES PVT. LTD.

1Y
Phone:+917249203006
Whatsapp: +91 7249203006
product: Tramadol EP Impurity E Tramadol Related Compound B ; 2-((dimethylamino)methyl)cyclohexan-1-one hydrochloride 42036-65-7 96%
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SHREE GANESH CHEMICALS

1Y
Phone:+91-8238386186
Whatsapp: +91 8238386186
product: 2-Dimethyl Amino methyl Cyclohexanone hydrochloride 99%
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DL INTRACHEM

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Phone:+91-9099014678
Whatsapp: +91-9099014678
product: 42036-65-7 98%
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