1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
- CAS NO.:95464-05-4
- Empirical Formula: C34H28Cl2FeP2Pd.CH2Cl2
- Molecular Weight: 816.63
- MDL number: MFCD00792899
- EINECS: 619-128-9
- SAFETY DATA SHEET (SDS)
- Update Date: 2025-01-27 09:38:02

What is 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex?
Chemical properties
orange/red solid
The Uses of 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
suzuki reaction
The Uses of 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex is used in the preparation of imidazoles, benzimidazoles, and tetrahydropyrimidines,it is also used as a catalyst for Suzuki and Stile couplings.
What are the applications of Application
[1,1′-Bis(diphenylphosphino)ferrocene]palladium(II) Dichloride Dichloromethane Adduct is a precurosor used in the preparation of imidazoles, benzimidazoles, and tetrahydropyrimidines
What are the applications of Application
1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex is an organometallic compound that can be used as a noble metal catalyst for carbonylation reactions, cross-coupling reactions, Suzuki reaction.
Synthesis
1. Dissolve 2.00 grams of sodium palladium chloride in 30mL of anhydrous ethanol to obtain the ethanol solution of sodium palladium chloride;
2. Dissolve 4.15 grams of 1,1 '-bis (diphenylphosphine) ferrocene in 41mL dichloromethane to obtain 1,1' -bis (diphenylphosphine) ferrocene dichloromethane solution;
3. Under stirring conditions, add the ethanol solution of sodium palladite chloride in step 1 to dichloromethane solution of 1, 1 '-bis (diphenylphosphine) ferrocene in step 2. Stir and react for 1h at 25℃. 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex crystal, yield 90.46%.
In this method, the target product 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex was synthesized directly with dichloromethane as the solvent in one step, eliminating the synthesis process of precursor PDCl2 (DPPF). The reaction process is simple, the synthesis cycle is short, easy to operate, and the purity of the synthesized product is 99.4%.
Properties of 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
Melting point: | 275-280 °C(lit.) |
Density | 1 g/cm3 |
storage temp. | Keep in dark place,Inert atmosphere,Room temperature |
solubility | Chloroform (Slightly), Methanol (Slightly) |
form | Powder |
color | orange-red |
Water Solubility | Insoluble in water. |
Stability: | Light Sensitive |
CAS DataBase Reference | 95464-05-4(CAS DataBase Reference) |
Safety information for 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
Signal word | Warning |
Pictogram(s) |
![]() Exclamation Mark Irritant GHS07 |
GHS Hazard Statements |
H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation H335:Specific target organ toxicity, single exposure;Respiratory tract irritation |
Precautionary Statement Codes |
P261:Avoid breathing dust/fume/gas/mist/vapours/spray. P280:Wear protective gloves/protective clothing/eye protection/face protection. P301+P312:IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for 1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex
1,1'-Bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex manufacturer
Vineeth Precious Catalysts Pvt. Ltd.
ASM Organics
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