R(+)-1-(PENTAFLUOROPHENYL)ETHANOL
Synonym(s):(R)-(+)-1-(Pentafluorophenyl)ethanol
- CAS NO.：104371-21-3
- Empirical Formula: C8H5F5O
- Molecular Weight: 212.12
- MDL number: MFCD00077839
- SAFETY DATA SHEET (SDS)
What is R(+)-1-(PENTAFLUOROPHENYL)ETHANOL?
Purification Methods
Recrystallise the ethanol from n-pentane at -40o and sublime it at 25o/0.3mm (use ice-cooled cold finger). It has also been purified by column chromatography through Kieselgel 60 (0.063-0.2mm mesh, Merck) and eluted with EtOAc/n-hexane (1:5), then recrystallised from n-pentane and sublimed in a vacuum. It has RF on Kieselgel 60 F254 TLC foil and eluting with EtOAc/n-hexane (1:5). [Meese Justus Liebigs Ann Chem 2004 1986.]
Properties of R(+)-1-(PENTAFLUOROPHENYL)ETHANOL
| Melting point: | 41-42 °C(lit.) |
| Boiling point: | 162.9±0.0 °C(Predicted) |
| Density | 1.498±0.06 g/cm3(Predicted) |
| Flash point: | 189 °F |
| pka | 13.14±0.20(Predicted) |
| optical activity | [α]20/D +7.0±0.5°, c = 1% in pentane |
| BRN | 5268492 |
Safety information for R(+)-1-(PENTAFLUOROPHENYL)ETHANOL
| Signal word | Warning |
| Pictogram(s) |
 Exclamation Mark Irritant GHS07 |
| GHS Hazard Statements |
H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation H335:Specific target organ toxicity, single exposure;Respiratory tract irritation |
| Precautionary Statement Codes |
P261:Avoid breathing dust/fume/gas/mist/vapours/spray. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for R(+)-1-(PENTAFLUOROPHENYL)ETHANOL
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