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HomeProduct name listN-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE

N-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE

N-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE Structural

What is N-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE?

Physical properties

bp 40–41 °C/10 mmHg; n20 D 1.4146.2

The Uses of N-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE

As bis-trimethylsilylated N-methylhydroxylamine N-Methyl-N,O-bis(trimethylsilyl)- hydroxylamine can convert aldehydes and ketones to N-methyl nitrones with regio- and chemoselectivity; source of methylnitrene by pyrolysis; source of the trimethylsilyl(methyl)aminyl radical by photolysis.

Preparation

It is obtained in 52% yield by reaction of Nmethylhydroxylamine with chlorotrimethylsilane (2.0 equiv) and triethylamine (3.3 equiv) in ether at 25 °C.

Properties of N-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE

Boiling point: 155.3±23.0 °C(Predicted)
Density  1.4146 g/cm3
storage temp.  Refrigerator
solubility  sol benzene, toluene, CH2Cl2, CHCl3.
form  clear liquid
pka 5.95±0.70(Predicted)
color  Colorless to Light yellow to Light orange

Safety information for N-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE

Signal word Danger
Pictogram(s)
ghs
Flame
Flammables
GHS02
ghs
Corrosion
Corrosives
GHS05
GHS Hazard Statements H226:Flammable liquids
H314:Skin corrosion/irritation
Precautionary Statement Codes P210:Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P233:Keep container tightly closed.
P240:Ground/bond container and receiving equipment.
P241:Use explosion-proof electrical/ventilating/lighting/…/equipment.
P242:Use only non-sparking tools.
P243:Take precautionary measures against static discharge.
P264:Wash hands thoroughly after handling.
P264:Wash skin thouroughly after handling.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P363:Wash contaminated clothing before reuse.
P301+P330+P331:IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353:IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P370+P378:In case of fire: Use … for extinction.
P405:Store locked up.
P403+P235:Store in a well-ventilated place. Keep cool.

Computed Descriptors for N-METHYL-N,O-BIS(TRIMETHYLSILYL)HYDROXYLAMINE

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