IODOMETHANE-D3
Synonym(s):Deuterated iodomethane;Methyl-12C,d3 iodide;Methyl-d3 Iodide
- CAS NO.：865-50-9
- Empirical Formula: CD3I
- Molecular Weight: 144.96
- MDL number: MFCD00001074
- EINECS: 212-744-5
- SAFETY DATA SHEET (SDS)
- Update Date: 2023-12-24 21:24:35
What is IODOMETHANE-D3?
Description
A deuterated form of iodomethane made from methanol-D4.IODOMETHANE-D3 is an important component in the organic synthesis of deuterium-labeled compounds.
Chemical properties
IODOMETHANE-D3 is a colorless liquid, sensitive to light and volatile.
The Uses of IODOMETHANE-D3
IODOMETHANE-D3 is used in the analysis of peptides and glycans using various analytical spectroscopic techniques.
The Uses of IODOMETHANE-D3
IODOMETHANE-D3 can be used as a methylating agent in organic synthesis.
Synthesis
An efficient method for the preparation of IODOMETHANE-D3, using METHANOL-D3 and iodine monomers as reaction materials, in a hydrogen atmosphere, with the addition of transition metal catalysts and ligands to produce IODOMETHANE-D3 in situ at 0°C-120°C.
Properties of IODOMETHANE-D3
| Melting point: | -66.5 °C(lit.) |
| Boiling point: | 42 °C(lit.) |
| Density | 2.330 g/mL at 25 °C |
| vapor density | 4.89 (vs air) |
| vapor pressure | 22.83 psi ( 55 °C) |
| refractive index | n |
| storage temp. | 0-6°C |
| solubility | Chloroform, Methanol (Slightly) |
| form | Liquid |
| color | Clear colorless |
| BRN | 1732026 |
| Stability: | Stable. Incompatible with strong bases, strong oxidizing agents. Moisture and light-sensitive. |
| EPA Substance Registry System | Methane-d3, iodo- (865-50-9) |
Safety information for IODOMETHANE-D3
| Signal word | Danger |
| Pictogram(s) |
 Skull and Crossbones Acute Toxicity GHS06  Health Hazard GHS08  Environment GHS09 |
| GHS Hazard Statements |
H312:Acute toxicity,dermal H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation H335:Specific target organ toxicity, single exposure;Respiratory tract irritation H351:Carcinogenicity H410:Hazardous to the aquatic environment, long-term hazard |
| Precautionary Statement Codes |
P273:Avoid release to the environment. P280:Wear protective gloves/protective clothing/eye protection/face protection. P301+P310:IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for IODOMETHANE-D3
| InChIKey | INQOMBQAUSQDDS-FIBGUPNXSA-N |
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product: 865-50-9 Iodomethane-d3 99%
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