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HomeProduct name listBromocyclohexane

Bromocyclohexane

Synonym(s):Cyclohexyl bromide

  • CAS NO.:108-85-0
  • Empirical Formula: C6H11Br
  • Molecular Weight: 163.06
  • MDL number: MFCD00003819
  • EINECS: 203-622-2
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-09-02 13:12:44
Bromocyclohexane Structural

What is Bromocyclohexane?

Chemical properties

colourless liquid

The Uses of Bromocyclohexane

Bromocyclohexane has been used to study the ionization of equatorial and axial conformational isomers of the chair-bromocyclohexane using vacuum ultraviolet mass-analyzed threshold ionization spectroscopy.

What are the applications of Application

Bromocyclohexane is used to study the ionization of equatorial and axial conformational isomers of the chair-bromocyclohexane

Preparation

Bromocyclohexane is synthesized by the reaction of cycloethanol and hydrobromic acid.

Synthesis Reference(s)

Canadian Journal of Chemistry, 50, p. 3109, 1972 DOI: 10.1139/v72-498
Journal of the American Chemical Society, 112, p. 8212, 1990 DOI: 10.1021/ja00178a080
The Journal of Organic Chemistry, 45, p. 1638, 1980 DOI: 10.1021/jo01297a020

General Description

Axial conformer of bromocyclohexane forms inclusion complexes with 9,9′-bianthryl and exhibits a weak 1,3 diaxial Cl...H interaction. It participates in the alkylation reaction of of para-xylene in the presence of graphite as catalyst to yield hydrocarbon.

Purification Methods

Shake the bromide with 60% aqueous HBr to remove the free alcohol. After removing excess HBr, the sample is dried and fractionally distilled. [IR: Roberts & Chambers J Am Chem Soc 73 5031 1951, Beilstein 5 III 48, 5 IV 67.]

Properties of Bromocyclohexane

Melting point: -57°C
Boiling point: 166-167 °C (lit.)
Density  1.324 g/mL at 25 °C (lit.)
vapor density  5.62 (vs air)
refractive index  n20/D 1.495(lit.)
Flash point: 145 °F
storage temp.  Sealed in dry,Room Temperature
solubility  Miscible with ethanol, ether, acetone, benzene and carbon tetrachloride.
form  Liquid
color  Clear colorless to light yellow
Specific Gravity approximate 1.33 (20℃)
Odor Unpleasant Odor
Water Solubility  insoluble
Sensitive  Air & Light Sensitive
Merck  14,2730
BRN  1098373
Dielectric constant 7.9(25℃)
Stability: Stable. Combustible. Incompatible with strong oxidizing agents, strong bases.
CAS DataBase Reference 108-85-0(CAS DataBase Reference)
NIST Chemistry Reference Cyclohexane, bromo-(108-85-0)
EPA Substance Registry System Cyclohexane, bromo- (108-85-0)

Safety information for Bromocyclohexane

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H227:Flammable liquids
H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P210:Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P261:Avoid breathing dust/fume/gas/mist/vapours/spray.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405:Store locked up.
P403+P235:Store in a well-ventilated place. Keep cool.
P501:Dispose of contents/container to..…

Computed Descriptors for Bromocyclohexane

InChIKey AQNQQHJNRPDOQV-UHFFFAOYSA-N

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