6-Bromoisoquinoline
- CAS NO.：34784-05-9
- Empirical Formula: C9H6BrN
- Molecular Weight: 208.05
- MDL number: MFCD04973299
- EINECS: 662-848-3
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-08-06 16:32:36
What is 6-Bromoisoquinoline?
What are the applications of Application
6-Bromoisoquinoline is a synthetic intermediate
Synthesis
Add the catalyst and p-bromoaniline to the dilute sulfuric acid, and add glycerol dropwise while controlling the temperature to 140-145°C. After the dropwise addition is completed, the dehydration reaction occurs at 140-145°C for 3 hours. Add the above reaction liquid dropwise to ice water, and then add ammonia water dropwise to adjust the pH of the system. Extract the reaction solution with toluene, concentrate the toluene phase at 150~155℃/15mmHg, and then distill the crude product to obtain the product 6-bromoisoquinoline.
Properties of 6-Bromoisoquinoline
| Melting point: | 44.0 to 48.0 °C |
| Boiling point: | 312.3±15.0 °C(Predicted) |
| Density | 1.564±0.06 g/cm3(Predicted) |
| Flash point: | >110℃ |
| storage temp. | Inert atmosphere,Room Temperature |
| solubility | DMF: 30 mg/ml; DMSO: 30 mg/ml; Ethanol: 30 mg/ml; Ethanol:PBS (pH 7.2) (1:8): .5 mg/ml |
| pka | 4.83±0.10(Predicted) |
| form | Crystalline Powder |
| color | White |
| λmax | 320nm(CHCl3)(lit.) |
| CAS DataBase Reference | 34784-05-9(CAS DataBase Reference) |
Safety information for 6-Bromoisoquinoline
| Signal word | Warning |
| Pictogram(s) |
 Exclamation Mark Irritant GHS07 |
| GHS Hazard Statements |
H302:Acute toxicity,oral H319:Serious eye damage/eye irritation |
| Precautionary Statement Codes |
P264:Wash hands thoroughly after handling. P264:Wash skin thouroughly after handling. P270:Do not eat, drink or smoke when using this product. P280:Wear protective gloves/protective clothing/eye protection/face protection. P301+P312:IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. P337+P313:IF eye irritation persists: Get medical advice/attention. |
Computed Descriptors for 6-Bromoisoquinoline
| InChIKey | ZTEATMVVGQUULZ-UHFFFAOYSA-N |
Abamectin manufacturer
JSK Chemicals
1Y
Phone:+91 9879767970;+919879767970
Whatsapp: +91 9879767970
product: 6-Bromoisoquinoline, 96% 99%
Dr. Silviu Pharmachem Pvt., Ltd.
1Y
Phone:+918390608382
Whatsapp: +91 8390608382
product: 6-Bromoisoquinoline 34784-05-9 98%
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