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HomeProduct name list4-Bromobiphenyl

4-Bromobiphenyl

  • CAS NO.:92-66-0
  • Empirical Formula: C12H9Br
  • Molecular Weight: 233.1
  • MDL number: MFCD00000100
  • EINECS: 202-176-6
  • Update Date: 2024-10-24 21:11:45
4-Bromobiphenyl Structural

What is 4-Bromobiphenyl?

Chemical properties

White powder

The Uses of 4-Bromobiphenyl

4-Bromobiphenyl is used as halogenated hydrocarbon and Intermediates of Liquid Crystals. It is also used in used in the synthesis of 4-biphenylthiolate.

The Uses of 4-Bromobiphenyl

4-Bromobiphenyl is used as a reagent in the synthesis of spirooxindole derivatives for use as AMPK activators.  It is also used as a reagent in the preparation of indenoindole derivatives as organic electroluminescent device materials.

What are the applications of Application

4-Bromobiphenyl is a halogenated hydrocarbon

General Description

Colorless crystals. Insoluble in water.

Air & Water Reactions

Insoluble in water.

Reactivity Profile

4-Bromobiphenyl may be sensitive to light, and it can react with oxidizing materials.

Fire Hazard

Combustible.

Synthesis

Into a 250 ml reactor equipped with magnetic agitation means, a condenser, a dropping funnel, and a thermometer, the following materials were introduced:
(i) 15.4 g biphenyl (0.1 M);
(ii) 100 ml solvent
at ambient temperature Then, over 10 min, the bromine was poured therein (39.2 g/0.22 M), whereupon the mixture was agitated for a varying period of time at ambient temperature. Upon completion of the reaction, the excess bromine was consumed by sodium or potassium sulfite or bisulfite. The organic phase was washed, dried and diluted to a given volume, and analyzed by CPG to give 4-Bromobiphenyl.

Purification Methods

Crystallise the biphenyl from abolute EtOH and dry it in vacuo.[Beilstein 5 IV 1819.]

Properties of 4-Bromobiphenyl

Melting point: 82-86 °C(lit.)
Boiling point: 310 °C(lit.)
Density  0.9327
refractive index  1.6565 (estimate)
Flash point: 143 °C
storage temp.  Sealed in dry,Room Temperature
solubility  dioxane: soluble1g/10 mL, clear, colorless to very faintly yellow
form  Crystalline Flakes
color  Almost white to slightly yellow
Water Solubility  Insoluble
BRN  1907453
Stability: Stable. Incompatible with oxidizing agents.
CAS DataBase Reference 92-66-0(CAS DataBase Reference)
NIST Chemistry Reference 1,1'-Biphenyl, 4-bromo-(92-66-0)
EPA Substance Registry System 4-Bromobiphenyl (92-66-0)

Safety information for 4-Bromobiphenyl

Signal word Danger
Pictogram(s)
ghs
Corrosion
Corrosives
GHS05
ghs
Exclamation Mark
Irritant
GHS07
ghs
Environment
GHS09
GHS Hazard Statements H302:Acute toxicity,oral
H315:Skin corrosion/irritation
H318:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
H400:Hazardous to the aquatic environment, acute hazard
Precautionary Statement Codes P273:Avoid release to the environment.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P391:Collect spillage. Hazardous to the aquatic environment

Computed Descriptors for 4-Bromobiphenyl

InChIKey PKJBWOWQJHHAHG-UHFFFAOYSA-N

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