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HomeProduct name list3,5-Dichlorobenzoyl chloride

3,5-Dichlorobenzoyl chloride

  • CAS NO.:2905-62-6
  • Empirical Formula: C7H3Cl3O
  • Molecular Weight: 209.46
  • MDL number: MFCD00009817
  • EINECS: 220-813-6
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-10-24 21:11:45
3,5-Dichlorobenzoyl chloride Structural

What is 3,5-Dichlorobenzoyl chloride?

Chemical properties

clear colorless to light yellow liquid or low

The Uses of 3,5-Dichlorobenzoyl chloride

3,5-Dichlorobenzoyl chloride is a useful intermediate for organic synthesis and other pharmaceutical processes.

The Uses of 3,5-Dichlorobenzoyl chloride

3,5-Dichlorobenzoyl chloride has been used in the preparation of:

  • N-(1,1-dimethylpropynyl)-3,5-dichlorobenzamide, herbicide
  • (3,5-dichlorophenyl)(2-(4-methoxyphenyl)-5-methylbenzofuran-3-yl)methanone

Flammability and Explosibility

Non flammable

Synthesis

3,5-Dichlorobenzoyl chloride is obtained by reacting by aryl carboxylic acid with DMF.Dissolve aryl carboxylic acid (10.0 mmol) in 50 mL DCM with drops of DMF to a 100 mL roundbottomed flask. Cool the mixture to 0°C. Add oxalyl chloride (20.0 mmol, 2.0 equivalents) dropwise to the reaction mixture. Allow the reaction mixture to react for another 4 hours. Concentrate the solvent in vacuo. Use the remaining residue directly.
synthetic method of 3,5-Dichlorobenzoyl chlorideFig The synthetic method of 3,5-Dichlorobenzoyl chloride

Properties of 3,5-Dichlorobenzoyl chloride

Melting point: 28 °C (lit.)
Boiling point: 135-137 °C/25 mmHg (lit.)
Density  135
vapor pressure  0.1 mm Hg ( 32 °C)
refractive index  n20/D 1.582(lit.)
Flash point: >230 °F
storage temp.  Refrigerator (+4°C)
solubility  soluble in Benzene,Toluene
form  powder to lump to clear liquid
color  White or Colorless to Almost white or Almost colorless
Sensitive  Moisture Sensitive
BRN  1940681
CAS DataBase Reference 2905-62-6(CAS DataBase Reference)
NIST Chemistry Reference 3,5-Dichlorobenzoyl chloride(2905-62-6)
EPA Substance Registry System Benzoyl chloride, 3,5-dichloro- (2905-62-6)

Safety information for 3,5-Dichlorobenzoyl chloride

Signal word Danger
Pictogram(s)
ghs
Corrosion
Corrosives
GHS05
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H302:Acute toxicity,oral
H314:Skin corrosion/irritation
Precautionary Statement Codes P260:Do not breathe dust/fume/gas/mist/vapours/spray.
P270:Do not eat, drink or smoke when using this product.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312:IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P303+P361+P353:IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for 3,5-Dichlorobenzoyl chloride

InChIKey GGHLXLVPNZMBQR-UHFFFAOYSA-N

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