2-Iodo-4-methoxy-1-nitrobenzene
- CAS NO.：214279-40-0
- Empirical Formula: C7H6INO3
- Molecular Weight: 279.03
- MDL number: MFCD01320682
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-05-10 08:45:28
What is 2-Iodo-4-methoxy-1-nitrobenzene?
Chemical properties
yellow to orange-brown crystals or
Synthesis
Silak reaction tube equipped with a magnetic stirrer was charged with 6.2 mg of silver sulfate,21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline,39.4 mg of 2-nitro-5-methoxybenzoic acid and 45 mg of sodium iodide4 mL of dimethyl sulfoxide. The reaction was heated at 160 ° C for 24 hours with oxygen. After the reaction, distilled water was added to quench the reaction. Extraction with ethyl acetate 3 times, each time 10mL. The combined organic phases are concentrated; 35.2 mg of 2-Iodo-4-methoxy-1-nitrobenzene was obtained in a yield of 63 percent.
Properties of 2-Iodo-4-methoxy-1-nitrobenzene
| Melting point: | 68-73 °C |
| Boiling point: | 352.1±27.0 °C(Predicted) |
| Density | 1.9259 (estimate) |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| form | Crystals or Crystalline Powder |
| color | Yellow to orange-brown |
| InChI | InChI=1S/C7H6INO3/c1-12-5-2-3-7(9(10)11)6(8)4-5/h2-4H,1H3 |
Safety information for 2-Iodo-4-methoxy-1-nitrobenzene
| Signal word | Warning |
| Pictogram(s) |
 Exclamation Mark Irritant GHS07 |
| GHS Hazard Statements |
H302:Acute toxicity,oral H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation H335:Specific target organ toxicity, single exposure;Respiratory tract irritation |
| Precautionary Statement Codes |
P261:Avoid breathing dust/fume/gas/mist/vapours/spray. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for 2-Iodo-4-methoxy-1-nitrobenzene
| InChIKey | NLTAHTYBZZSCIT-UHFFFAOYSA-N |
| SMILES | C1([N+]([O-])=O)=CC=C(OC)C=C1I |
New Products
Tert-butyl bis(2-chloroethyl)carbamate (S)-3-Aminobutanenitrile hydrochloride N-Boc-D-alaninol N-BOC-D/L-ALANINOL N-octanoyl benzotriazole 3,4-Dibenzyloxybenzaldehyde 4-Hydrazinobenzoic acid 1,1’-CARBONYLDIIMIDAZOLE R-2-BENZYLOXY PROPIONIC ACID 4-HYDROXY BENZYL ALCOHOL 1,1’-CARBONYLDI (1,2-4 TRIAZOLE) 3-NITRO-2-METHYL ANILINE (2-Hydroxyphenyl)acetonitrile 4-Bromopyrazole 5-BROMO-2CYANO PYRIDINE 5,6-Dimethoxyindanone 5-broMo-2-chloro-N-cyclopentylpyriMidin-4-aMine 2-(Cyanocyclohexyl)acetic acid 4-methoxy-3,5-dinitropyridine 2-aminopropyl benzoate hydrochloride 1-(4-(aminomethyl)benzyl)urea hydrochloride tert-butyl 4- (ureidomethyl)benzylcarbamate diethyl 2-(2-((tertbutoxycarbonyl)amino) ethyl)malonate Ethyl-2-chloro((4-methoxyphenyl)hydrazono)acetateRelated products of tetrahydrofuran
You may like
-
214279-40-0 3-iodo -4-nitro anisole 98%View Details
214279-40-0 -
2-Iodo-4-methoxy-1-nitrobenzene CAS 214279-40-0View Details
214279-40-0 -
55441-95-7 99%View Details
55441-95-7 -
N-Vinylformamide 99%View Details
13162-05-5 -
Chloro Uracil 1820-81-1 99%View Details
1820-81-1 -
2-ethyl-6-methyl-3-hydroxypyridine succinate 99%View Details
127464-43-1 -
2-ETHYLPYRIDINE 100-71-0 99%View Details
100-71-0 -
181228-33-1 (S)-Methyl 3-amino-2-((tert-butoxycarbonyl)amino)propanote Hydrochloride (DAP-OMe. HCl) 99%View Details
181228-33-1
Statement: All products displayed on this website are only used for non medical purposes such as industrial applications or scientific research, and cannot be used for clinical diagnosis or treatment of humans or animals. They are not medicinal or edible.