2-Iodo-4-methoxy-1-nitrobenzene
- CAS NO.:214279-40-0
- Empirical Formula: C7H6INO3
- Molecular Weight: 279.03
- MDL number: MFCD01320682
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-05-10 08:45:28
What is 2-Iodo-4-methoxy-1-nitrobenzene?
Chemical properties
yellow to orange-brown crystals or
Synthesis
Silak reaction tube equipped with a magnetic stirrer was charged with 6.2 mg of silver sulfate,21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline,39.4 mg of 2-nitro-5-methoxybenzoic acid and 45 mg of sodium iodide4 mL of dimethyl sulfoxide. The reaction was heated at 160 ° C for 24 hours with oxygen. After the reaction, distilled water was added to quench the reaction. Extraction with ethyl acetate 3 times, each time 10mL. The combined organic phases are concentrated; 35.2 mg of 2-Iodo-4-methoxy-1-nitrobenzene was obtained in a yield of 63 percent.
Properties of 2-Iodo-4-methoxy-1-nitrobenzene
Melting point: | 68-73 °C |
Boiling point: | 352.1±27.0 °C(Predicted) |
Density | 1.9259 (estimate) |
storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
form | Crystals or Crystalline Powder |
color | Yellow to orange-brown |
InChI | InChI=1S/C7H6INO3/c1-12-5-2-3-7(9(10)11)6(8)4-5/h2-4H,1H3 |
Safety information for 2-Iodo-4-methoxy-1-nitrobenzene
Signal word | Warning |
Pictogram(s) |
Exclamation Mark Irritant GHS07 |
GHS Hazard Statements |
H302:Acute toxicity,oral H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation H335:Specific target organ toxicity, single exposure;Respiratory tract irritation |
Precautionary Statement Codes |
P261:Avoid breathing dust/fume/gas/mist/vapours/spray. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for 2-Iodo-4-methoxy-1-nitrobenzene
InChIKey | NLTAHTYBZZSCIT-UHFFFAOYSA-N |
SMILES | C1([N+]([O-])=O)=CC=C(OC)C=C1I |
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