(2S)-(+)-1-BENZOYL-2-TERT-BUTYL-3-METHYL-4-IMIDAZOLIDINONE
- CAS NO.：101055-56-5
- Empirical Formula: C15H20N2O2
- Molecular Weight: 260.33
- MDL number: MFCD00040620
- SAFETY DATA SHEET (SDS)
What is (2S)-(+)-1-BENZOYL-2-TERT-BUTYL-3-METHYL-4-IMIDAZOLIDINONE?
Purification Methods
Recrystallise these chiral imidazolinones from boiling EtOH (solubility is 1.43g/mL) or better by dissolving in CH2Cl2 and adding pentane, filtering and drying for at least 12hours at 60o/0.1mm and sublime them at 135o/0.01mm. They have also been purified by flash column chromatography through Merck silica gel at 0.04-0.063mm and using Et2O/pet ether/MeOH (60:35:5) as eluent. They are then recrystallised from EtOH/pet ether. [IR, NMR: Seebach et al. Helv Chim Acta 70 237 1987, Fitzi & Seebach Angew Chem, Int Ed Engl 25 345 1986.] The racemate is purified in a similar manner and has m 104-105o [NMR: Seebach et al. Helv Chim Acta 68 949 1985].
Properties of (2S)-(+)-1-BENZOYL-2-TERT-BUTYL-3-METHYL-4-IMIDAZOLIDINONE
| Melting point: | 145-147 °C |
| storage temp. | 2-8°C |
Safety information for (2S)-(+)-1-BENZOYL-2-TERT-BUTYL-3-METHYL-4-IMIDAZOLIDINONE
Computed Descriptors for (2S)-(+)-1-BENZOYL-2-TERT-BUTYL-3-METHYL-4-IMIDAZOLIDINONE
New Products
4-AMINO-TETRAHYDRO-PYRAN-4-CARBOXYLIC ACID HCL 4-(Dimethylamino)tetrahydro-2H-pyran-4-carbonitrile 4-Aminotetrahydropyran-4-carbonitrile Hydrochloride (R)-3-Aminobutanenitrile Hydrochloride 3-((Dimethylamino)methyl)-5-methylhexan-2-one oxalate 1,4-Dioxa-8-azaspiro[4.5]decane 5-Bromo-2-nitropyridine Nimesulide BP Aceclofenac IP/BP/EP Diclofenac Sodium IP/BP/EP/USP Mefenamic Acid IP/BP/EP/USP Ornidazole IP Diclofenac Potassium THOMAIND PAPER PH 2.0 TO 4.5 1 BOX BUFFER CAPSULE PH 9.2 - 10 CAP SODIUM CHLORIDE 0.1N CVS ALLOXAN MONOHYDRATE 98% PLATINUM 0.5% ON 3 MM ALUMINA PELLETS (TYPE 73) LITHIUM AAS SOLUTION 2-Bromo-1-(bromomethyl)-3-chloro-5-nitrobenzene 2-Bromo-3-nitroaniline N-(3-Hydroxypropyl)-N-methylacetamide 3-Bromo-6-chloropyridazine 4-ethyl-3-nitrobenzoic acidRelated products of tetrahydrofuran
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