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HomeProduct name list2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine

2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine

2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine Structural

What is 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine?

Chemical properties

white solid powder

Synthesis

The compound, 2-chloro-4,6-diphenyl-1,3,5-triazine (50 g, 187 mmol) was dissolved in THF (1 L) under a nitrogen environment, (4-bromophenyl)boronic acid (45 g, 224.12 mmol, Aldrich Corporation), and tetrakis(triphenylphosphine)palladium (2.1 g, 1.87 mmol) were added thereto, and the mixture was stirred. Potassium carbonate saturated in water (64 g, 467 mmol) was added thereto, and the obtained mixture was heated and refluxed at 80° C. for 12 hours. When the reaction was complete, water was added to the reaction solution, and the mixture was extracted with dichloromethane (DCM) and then, filtered after removing moisture with anhydrous MgSO4 and concentrated under a reduced pressure. This obtained residue was separated and purified through flash column chromatography to obtain 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine (70 g and 96%).

Properties of 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine

Melting point: 200.0 to 204.0 °C
Boiling point: 573.9±52.0 °C(Predicted)
Density  1.381
storage temp.  Sealed in dry,Room Temperature
form  powder to crystal
pka 0.45±0.10(Predicted)
color  White to Almost white

Safety information for 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
Precautionary Statement Codes P264:Wash hands thoroughly after handling.
P264:Wash skin thouroughly after handling.
P280:Wear protective gloves/protective clothing/eye protection/face protection.

Computed Descriptors for 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine

InChIKey AYHGAQGOMUQMTR-UHFFFAOYSA-N

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