2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
- CAS NO.:23449-08-3
- Empirical Formula: C21H14BrN3
- Molecular Weight: 388.26
- MDL number: MFCD00194632
- SAFETY DATA SHEET (SDS)
- Update Date: 2023-11-21 15:09:27
What is 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine?
Chemical properties
white solid powder
Synthesis
The compound, 2-chloro-4,6-diphenyl-1,3,5-triazine (50 g, 187 mmol) was dissolved in THF (1 L) under a nitrogen environment, (4-bromophenyl)boronic acid (45 g, 224.12 mmol, Aldrich Corporation), and tetrakis(triphenylphosphine)palladium (2.1 g, 1.87 mmol) were added thereto, and the mixture was stirred. Potassium carbonate saturated in water (64 g, 467 mmol) was added thereto, and the obtained mixture was heated and refluxed at 80° C. for 12 hours. When the reaction was complete, water was added to the reaction solution, and the mixture was extracted with dichloromethane (DCM) and then, filtered after removing moisture with anhydrous MgSO4 and concentrated under a reduced pressure. This obtained residue was separated and purified through flash column chromatography to obtain 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine (70 g and 96%).
Properties of 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
Melting point: | 200.0 to 204.0 °C |
Boiling point: | 573.9±52.0 °C(Predicted) |
Density | 1.381 |
storage temp. | Sealed in dry,Room Temperature |
form | powder to crystal |
pka | 0.45±0.10(Predicted) |
color | White to Almost white |
Safety information for 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
Signal word | Warning |
Pictogram(s) |
Exclamation Mark Irritant GHS07 |
GHS Hazard Statements |
H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation |
Precautionary Statement Codes |
P264:Wash hands thoroughly after handling. P264:Wash skin thouroughly after handling. P280:Wear protective gloves/protective clothing/eye protection/face protection. |
Computed Descriptors for 2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine
InChIKey | AYHGAQGOMUQMTR-UHFFFAOYSA-N |
New Products
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