Di-tert-butyl iminodicarboxylate Bis(tert-butoxycarbonyl)amine

Di-tert-butyl iminodicarboxylate COA TDS price MSDS

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Di-tert-butyl iminodicarboxylate CAS 51779-32-9

Bis(tert-butoxycarbonyl)amine CAS 51779-32-9

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Di-tert-butyl iminodicarboxylate Chemical Properties
Melting point     114-117 °C(lit.)
storage temp.     2-8°C
form     Crystalline Powder
color     White to beige
Water Solubility     Insoluble in water.
HS Code     29241990
MSDS Information
Di-tert-butyl iminodicarboxylate Usage And Synthesis
Chemical Properties    White to beige crystalline powder
Di-tert-butyl iminodicarboxylate Preparation Products And Raw materials
Product Name:    Di-tert-butyl iminodicarboxylate
Synonyms:    (BOC)2NH FLUKA;Bis(tert-butoxycarbonyl)amine;IMINODICARBOXYLIC ACID DI-TERT-BUTYL ESTER;LABOTEST-BB LT00233154;DI-T-BUTYL IMINODICARBOXYLATE;DI-TERT-BUTYL IMINODICARBOXYLATE;DI-TERT-BUTYL IMIDODICARBONATE;N-BOC-TERT-BUTYLCARBAMATE
CAS:    51779-32-9
MF:    C10H19NO4
MW:    217.26
Di-tert-butyl-iminodicarboxylate is an organic compound that can be described with the formula [(CH3)3COC(O)]2NH. It is a white solid that is soluble in organic solvents. The compound is used as a reagent for the preparation of primary amines from alkyl halides. It was popularized as an alternative to the Gabriel synthesis for the same conversion. Amines can also be prepared from alcohols by dehydration using the Mitsunobu reaction.
In the usual implementation the reagent is deprotonated to give the potassium salt, which is N-alkylated. The Boc protecting groups are subsequently removed under acidic conditions.
Appearance & Physical State     WHITE TO FAINT YELLOW POWDER
Density     1.037 g/cm3
Boiling Point     273.8ºC at 760 mmHg
Melting Point     114-117ºC
Flash Point     119.4ºC
Refractive Index     1.442
Storage Condition     2-8ºC
tert-butyl N-[(2-methylpropan-2-yl)oxycarbonyl]carbamate; tert-Butyl iminodicarboxylate; N-Boc-tert-butylcarbamate; Iminodicarboxylic Acid Di-tert-butyl Ester;
Di-tert-butyl iminodicarboxylate; Iminodicarboxylic acid di-tert-butyl ester; (BOC)2NH; Bis(tert-butoxycarbonyl)ammonia; N-Boc-tert-butylcarbamate; Imidodicarbonic acid, C,C'-bis(1,1-dimethylethyl) ester; di-tert-butyl imidodicarbonate; Di-t-butyl iminodicarbonate