N-Phenyl-bis(trifluoromethanesulfonimide) 37595-74-7

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N-Phenyl-bis(trifluoromethanesulfonimide) CAS 37595-74-7

N,N-Bis(trifluoromethylsulfonyl)aniline CAS 37595-74-7

Appearance: white to off-white crystalline powder

Name:    N-Phenyl-bis(trifluoromethanesulfonimide)
Synonyms:    PHENYL TRIFLIMIDE;N,N-Bis(trifluoromethanesulphonyl)aniline~Phenyl triflimide~N-Phenyltrifluoromethanesulphonimide;Phenyl triflimide~N-Phenyltrifluoromethanesulphonimide;N-PHENYL-BIS-(TRIFLUORMETHANSULFONIMID);N,N-BIS-(TRIFLUOROMETHANESULFONYL)ANILINE;1,1,1-Trifluoro-N-phenyl-N-(trifluoromethyl)sulphonylmethanesulphonamide;N-Phenylbis(trifluoromethanesulphonimide)97%;n-phenylbis(trifluorometanesulfonimide)
CAS:    37595-74-7
MF:    C8H5F6NO4S2
MW:    357.25
EINECS:    609-445-0
Product Categories:    API intermediates;-
Mol File:    37595-74-7.mol
N-Phenyl-bis(trifluoromethanesulfonimide) Structure
N-Phenyl-bis(trifluoromethanesulfonimide) Chemical Properties
Melting point     100-102 °C(lit.)
solubility     Soluble in methanol. Slightly soluble in chloroform and ethyl acetate.

 N-Phenylbis(trifluoromethanesulfonamide) is used in the enantioselective synthesis of β-amino acids via the Mannich reaction. Used in the synthesis of sphingosine 1-phosphate-1 receptor agonists useful in pharmaceutical application.
Phenyl Triflimide
Synonyms          

1,1,1-Trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]methanesulfonamide;N-Phenyl-N-[(trifluoromethyl)sulfonyl]trifluoromethanesulfonamide;N-Phenylbis(trifluoromethanesulfonimide);N-Phenyltriflimide;N-Phenyltrifluoromethylsulfonimide;Phenyl triflimide;Trifluoro-N-phenyl-N-[(trifluoromethyl)sulfonyl]methanesulfonamide;N-Phenylbis(trifluoromethanesulphonimide); 1,1,1-Trifluoro-N-phenyl-N-trifluoromethanesulfonylmethanesulfonamide; N-Phenyl-bis(trifluoromethanesulfonimide); PhNTf2; N-Phenyltrifluoromethanesulfonimide; N-Phenyl-N-[(trifluoromethyl)sulfonyl]trifluoromethanesulfonamide;
Appearance & Physical State     white to off-white crystalline powder
Density     1.766 g/cm3
Boiling Point     305.3ºC at 760 mmHg
Melting Point     100-102ºC
Flash Point     138.4ºC
Refractive Index     1.488
Safety Info
Safety Statements     S26-S36
WGK Germany     3
Risk Statements     R36/37/38

form     Crystals or Crystalline Powder
color     White or colorless
Sensitive     Moisture Sensitive
BRN     1269141
InChIKey    DIOHEXPTUTVCNX-UHFFFAOYSA-N
CAS DataBase Reference    37595-74-7(CAS DataBase Reference)
NIST Chemistry Reference    N-phenyltrifluoromethanesulfonimide(37595-74-7)
Safety Information
Hazard Codes     Xi
Risk Statements     36/37/38
Safety Statements     26-36
WGK Germany     3
F     21
Hazard Note     Irritant
HazardClass     IRRITANT
HS Code     29242100
MSDS Information

N-Phenyl-bis(trifluoromethanesulfonimide) Usage And Synthesis
Chemical Properties    white to off-white crystalline powder
Uses    N-Phenylbis(trifluoromethanesulfonamide) is used in the enantioselective synthesis of β-amino acids via the Mannich reaction. Used in the synthesis of sphingosine 1-phosphate-1 receptor agonists usefu l in pharmaceutical application.
N-Phenyl-bis(trifluoromethanesulfonimide) Preparation Products And Raw materials
Raw materials    Etanol-->Sodium hydroxide-->Tetrahydrofuran-->Dichloromethane-->Potassium carbonate-->Magnesium sulfate-->Triethylamine-->Sodium chloride-->Sodium hydride -->Aniline-->Trifluoromethanesulfonic anhydride-->TRIFLUOROMETHANESULFONYL CHLORIDE