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Homecompany3,3',4,4'-Benzophenonetetracarboxylic dianhydride
3,3',4,4'-Benzophenonetetracarboxylic dianhydride
3,3',4,4'-Benzophenonetetracarboxylic dianhydride

3,3',4,4'-Benzophenonetetracarboxylic dianhydride

Price USD1.00
Packge 1kg
  • Min. Order:1kg
  • Supply Ability:100KG
  • Time:2019-07-06

Product Details

  • Product Name3,3',4,4'-Benzophenonetetracarboxylic dianhydride
  • CAS No.2421-28-5
  • EINECS No.219-348-1
  • MFC17H6O7
  • MW322.23
  • InChIKeyVQVIHDPBMFABCQ-UHFFFAOYSA-N
  • AppearanceNeedles or Crystalline PowderOff-white to brown
  • Boiling point 320°C 5mm
  • density 1,57 g/cm3
  • Water Solubility REACTS
  • Melting point 218-222 °C (lit.)
  • storage temp. Inert atmosphere,Room Temperature
 
3,3',4,4'-Benzophenonetetracarboxylic dianhydride Basic information
Product Name: 3,3',4,4'-Benzophenonetetracarboxylic dianhydride
Synonyms: 1,3-Isobenzofurandione, 5,5'-carbonylbis-;3,3',4,4'-Benzophenonetetracarboxylic acid dianhydride;3,3',4,4'-Tetracarboxybenzophenone dianhydride;3,3’,4,4’-benzophenonetetracarboxylicaciddianhydride;3-Isobenzofurandione,5,5’-carbonylbis-1;4,4'-Carbonylbis[phthalic anhydride];4,4'-Diphthalic anhydride ketone;5,5’-carbonylbis-3-isobenzofurandione
CAS: 2421-28-5
MF: C17H6O7
MW: 322.23
EINECS: 219-348-1
Product Categories: pharmacetical;Aromatic Tetracarboxylic Dianhydrides (for High-Performance Polymer Research);Benzophenones (for High-Performance Polymer Research);Functional Materials;Reagent for High-Performance Polymer Research;fine chemicals, specialty chemicals, intermediates, electronic chemical, organic synthesis, pharmaceutical intermediates;fine chemicals, specialty chemicals, intermediates, electronic chemical, organic synthesis, functional materials
Mol File: 2421-28-5.mol
3,3',4,4'-Benzophenonetetracarboxylic dianhydride Structure
 
3,3',4,4'-Benzophenonetetracarboxylic dianhydride Chemical Properties
Melting point  218-222 °C(lit.)
Boiling point  320°C 5mm
density  1,57 g/cm3
vapor density  1.4 (vs air)
vapor pressure  <0.1 mm Hg ( 0 °C)
refractive index  1.6380 (estimate)
Fp  324 °C
solubility  DMF: 0.1 g/mL, clear
form  Needles or Crystalline Powder
color  Off-white to brown
explosive limit 16%
Water Solubility  REACTS
Sensitive  Moisture Sensitive
λmax 580nm(CH3CN)(lit.)
Sublimation  220-230 ºC
BRN  761777
NIST Chemistry Reference Bis-(3-phthalyl anhydride) ketone(2421-28-5)
EPA Substance Registry System 1,3-Isobenzofurandione, 5,5'-carbonylbis-(2421-28-5)
 
Safety Information
Hazard Codes  Xi
Risk Statements  36/37
Safety Statements  25
WGK Germany  1
21
TSCA  Yes
HS Code  29183000
MSDS Information
Provider Language
BTDA English
ACROS English
SigmaAldrich English
ALFA English
 
3,3',4,4'-Benzophenonetetracarboxylic dianhydride Usage And Synthesis
Chemical Properties white crystall powder
Uses BTDA is important monomer of polyimide, and used for production of polyimide material. The material has high temperature resistance, low temperature resistance, corrosion resistance, radiation resistance, insulation, shock resistance, excellent performance. Can be made into structure parts, laminates, films, adhesives, coatings, insulation materials and reinforcing material, etc., can be widely used in the field of aerospace, electrical / electronics, shipbuilding, automobile, precision machinery.
Uses Used in the synthesis of polyimides.
Purification Methods The main impurity is the free acid formed by hydrolysis (check for OH bands in the IR). This can be converted to the dianhydride by treating with Ac2O (molar ratio of 4 to 1 of acid), heating at 110-120o for 1.5 to 2hours, cooling to 0—5o and collecting the dianhydride. This is then dissolved in hot dioxane or Me2CO, filtered and cooled to 10—15o. The moisture sensitive solid is collected and dried at 120—130o in vacuo. It has been sublimed at high vacuum. [Faberov et al. J Org Chem USSR 4 153 (English translation) 1968.]

Company Profile Introduction

Henan CoreyChem Co., Ltd, based on the original Zhengzhou Cote Chemical Research Institute, be brave in absorbing highly educated talents & overseas returnees; actively responded to Zhengzhou City High-tech Zone Government’s Special Care Policy, reorganized and founded in National University of Science and Technology Park, which is a high-tech, stock enterprise of high-end chemical Custom synthesis;The park was created by the People's Government of Henan Province, and proved by Ministry of Education and the National Science & Technology, taking the construction mode of "many college a park, and common development", mainly depends on Zhengzhou University and Henan University’s scientific research and talent advantage to set up Universities, scientific research institute and enterprise scientific research achievements transformation platform, to make high-tech enterprises incubate,  is the new high-tech talent gathering base, high and new technology industry enterprise radiation base, colleges and universities technological innovation base.
 
Henan Coreychem Co., Ltd, facing global High-tech pharmaceutical raw materials, high complex new type intermediates, fine chemicals custom synthesis, scale-up production and Rare chemicals trade. Corey have well-equipped machine, strong technical force and considerate marketing team service. We also have rich experience advantage in basic research, small scale process development, scale-up, industrial technology development & production and cost control.
 
  • Since:2014-12-17
  • Address: No.967,15th Floor,Unit 7, Building 1, No.70 of DianChang Road, High-tech Development Zone, Zhengzho
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