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TFEC

TFEC Structural

What is TFEC?

Preparation

A solution of 2,2,2-trifluoroethanol (200 g, 2.0 mol) and pyridine (158 g, 2.0 mol) in dry diethyl ether (1 L) was treated with phosgene (99 g, 1.0 mol). The reaction mixture was stirred overnight and then filtered. The filtrate was distilled to give 199 g (88%) of bis(2,2,2-trifluoroethyl) carbonate.

Properties of TFEC

Boiling point: 118°C(lit.)
Density  1.470±0.06 g/cm3(Predicted)
refractive index  1.3120 to 1.3160
solubility  Chloroform (Soluble), Methanol (Slightly)
form  clear liquid
color  Colorless to Almost colorless

Safety information for TFEC

Signal word Warning
Pictogram(s)
ghs
Flame
Flammables
GHS02
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H226:Flammable liquids
H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P210:Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P241:Use explosion-proof electrical/ventilating/lighting/…/equipment.
P261:Avoid breathing dust/fume/gas/mist/vapours/spray.

Computed Descriptors for TFEC

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