tert-Butyl phenyl carbonate
- CAS NO.：6627-89-0
- Empirical Formula: C11H14O3
- Molecular Weight: 194.23
- MDL number: MFCD00008804
- EINECS: 229-601-8
- SAFETY DATA SHEET (SDS)
- Update Date: 2023-06-08 17:06:38
What is tert-Butyl phenyl carbonate?
Chemical properties
Clear light yellow liquid
The Uses of tert-Butyl phenyl carbonate
tert-Butyl phenyl carbonate is used in determination of octanol-water partition coefficients by microemulsion electrokinetic chromatography. It is also used in the synthesis of 2-nitroindoles and as a reagent for mono-Boc protection of α,ω-diamines.
What are the applications of Application
tert-Butyl phenyl carbonate is a reagent for mono-Boc protection of α,ω-diamines
Purification Methods
If IR is free from OH, then purify it by redistillation; otherwise dissolve it in Et2O, wash it with 5% HCl, then H2O, dry it (MgSO4), evaporate and distil it through a Claisen head under vacuum. Care should be taken as distillation of large quantities can lead to decomposition with liberation of CO2 and isobutylene; use the necessary precautions. [Carpino J Am Chem Soc 79 98 1957, Beilstein 6 IV 629.]
Properties of tert-Butyl phenyl carbonate
| Boiling point: | 83 °C/0.6 mmHg (lit.) |
| Density | 1.05 g/mL at 20 °C (lit.) |
| refractive index | n |
| Flash point: | 214 °F |
| storage temp. | Inert atmosphere,Room Temperature |
| solubility | Chloroform (Slightly) |
| form | Liquid or Low Melting Solid |
| color | Colorless |
| Water Solubility | Slightly soluble in water. |
| BRN | 2361602 |
| NIST Chemistry Reference | Carbonic acid 1,1-dimethylethyl ester(6627-89-0) |
Safety information for tert-Butyl phenyl carbonate
| Signal word | Warning |
| Pictogram(s) |
 Exclamation Mark Irritant GHS07 |
| GHS Hazard Statements |
H315:Skin corrosion/irritation H319:Serious eye damage/eye irritation H335:Specific target organ toxicity, single exposure;Respiratory tract irritation |
| Precautionary Statement Codes |
P261:Avoid breathing dust/fume/gas/mist/vapours/spray. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for tert-Butyl phenyl carbonate
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product: 6627-89-0 tert-butyl phenyl carbonate 98%
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