Diethyl 1,1-cyclopropanedicarboxylate
- CAS NO.：1559-02-0
- Empirical Formula: C9H14O4
- Molecular Weight: 186.21
- MDL number: MFCD00001283
- EINECS: 216-321-6
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-11-01 18:09:03
What is Diethyl 1,1-cyclopropanedicarboxylate?
Chemical properties
clear colorless liquid
The Uses of Diethyl 1,1-cyclopropanedicarboxylate
Diethyl 1,1-Cyclopropanedicarboxylate (cas# 1559-02-0) is a compound useful in organic synthesis.
Synthesis Reference(s)
Synthesis, p. 690, 1980 DOI: 10.1055/s-1980-29171
General Description
Diethyl cyclopropane-1,1-dicarboxylate participates in ring-opening addition reactions with various nucleophilic reagents.
Purification Methods
If it is free from OH bands in the IR, then fractionally distil the ester and redistil the middle fraction. Otherwise shake it with aqueous NaHCO3, dry it (MgSO4), filter and distil as before or re-esterify it. [As synthon see Danishefsky Acc Chem Res 12 66 1979, Beilstein 9 I 314, 9 II 512, 9 III 3595, 9 IV 2786.]
Properties of Diethyl 1,1-cyclopropanedicarboxylate
| Melting point: | 134-136 °C(lit.) |
| Boiling point: | 94-96 °C/10 mmHg (lit.) |
| Density | 1.055 g/mL at 25 °C (lit.) |
| refractive index | n |
| Flash point: | 188 °F |
| storage temp. | Sealed in dry,Room Temperature |
| solubility | Acetone (Slightly), Chlorform (Slightly), Methanol (Slightly) |
| form | Liquid |
| color | Clear colorless |
| BRN | 2049509 |
| CAS DataBase Reference | 1559-02-0(CAS DataBase Reference) |
| NIST Chemistry Reference | Diethyl 1,1-cyclopropanedicarboxylate(1559-02-0) |
Safety information for Diethyl 1,1-cyclopropanedicarboxylate
| Signal word | Warning |
| Pictogram(s) |
 Exclamation Mark Irritant GHS07 |
| GHS Hazard Statements |
H227:Flammable liquids |
| Precautionary Statement Codes |
P210:Keep away from heat/sparks/open flames/hot surfaces. — No smoking. P280:Wear protective gloves/protective clothing/eye protection/face protection. P370+P378:In case of fire: Use … for extinction. P403+P235:Store in a well-ventilated place. Keep cool. P501:Dispose of contents/container to..… |
Computed Descriptors for Diethyl 1,1-cyclopropanedicarboxylate
Diethyl 1,1-cyclopropanedicarboxylate manufacturer
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