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HomeProduct name listDiethyl 1,1-cyclopropanedicarboxylate

Diethyl 1,1-cyclopropanedicarboxylate

  • CAS NO.:1559-02-0
  • Empirical Formula: C9H14O4
  • Molecular Weight: 186.21
  • MDL number: MFCD00001283
  • EINECS: 216-321-6
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-11-01 18:09:03
Diethyl 1,1-cyclopropanedicarboxylate Structural

What is Diethyl 1,1-cyclopropanedicarboxylate?

Chemical properties

clear colorless liquid

The Uses of Diethyl 1,1-cyclopropanedicarboxylate

Diethyl 1,1-Cyclopropanedicarboxylate (cas# 1559-02-0) is a compound useful in organic synthesis.

Synthesis Reference(s)

Synthesis, p. 690, 1980 DOI: 10.1055/s-1980-29171

General Description

Diethyl cyclopropane-1,1-dicarboxylate participates in ring-opening addition reactions with various nucleophilic reagents.

Purification Methods

If it is free from OH bands in the IR, then fractionally distil the ester and redistil the middle fraction. Otherwise shake it with aqueous NaHCO3, dry it (MgSO4), filter and distil as before or re-esterify it. [As synthon see Danishefsky Acc Chem Res 12 66 1979, Beilstein 9 I 314, 9 II 512, 9 III 3595, 9 IV 2786.]

Properties of Diethyl 1,1-cyclopropanedicarboxylate

Melting point: 134-136 °C(lit.)
Boiling point: 94-96 °C/10 mmHg (lit.)
Density  1.055 g/mL at 25 °C (lit.)
refractive index  n20/D 1.433(lit.)
Flash point: 188 °F
storage temp.  Sealed in dry,Room Temperature
solubility  Acetone (Slightly), Chlorform (Slightly), Methanol (Slightly)
form  Liquid
color  Clear colorless
BRN  2049509
CAS DataBase Reference 1559-02-0(CAS DataBase Reference)
NIST Chemistry Reference Diethyl 1,1-cyclopropanedicarboxylate(1559-02-0)

Safety information for Diethyl 1,1-cyclopropanedicarboxylate

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H227:Flammable liquids
Precautionary Statement Codes P210:Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P370+P378:In case of fire: Use … for extinction.
P403+P235:Store in a well-ventilated place. Keep cool.
P501:Dispose of contents/container to..…

Computed Descriptors for Diethyl 1,1-cyclopropanedicarboxylate

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