DESYL CHLORIDE
- CAS NO.：447-31-4
- Empirical Formula: C14H11ClO
- Molecular Weight: 230.69
- MDL number: MFCD00000858
- EINECS: 207-181-7
- SAFETY DATA SHEET (SDS)
- Update Date: 2024-07-29 17:07:33
What is DESYL CHLORIDE?
Chemical properties
off-white to light beige powder
Purification Methods
For the purification of small quantities recrystallise it from pet ether (b 40-60o), but use MeOH or EtOH for larger quantities. For the latter solvent, dissolve 12.5g of chloride in 45mL of boiling EtOH (95%), filter and the filtrate yields colourless crystals (7.5g) on cooling. A further crop (0.9g) can be obtained by cooling in an ice-salt bath. It turns brown on exposure to sunlight but it is stable in sealed dark containers. The R(+)-enantiomer has m 75-76o (from pet ether) and []546.1 +168.4o (c 0.6, Me2CO) [Roger & Wood J Chem Soc 811 1954]. [Henley & Turner J Chem Soc 1182 1931, Ward Org Synth Coll Vol II 159 1943, Beilstein 7 H 436, 7 I 234, 7 II 369, 7 III 2106, 7 IV 1396.]
Properties of DESYL CHLORIDE
| Melting point: | 62-63 °C(lit.) |
| Boiling point: | 330°C (rough estimate) |
| Density | 1.1223 (rough estimate) |
| refractive index | 1.5260 (estimate) |
| storage temp. | Store below +30°C. |
| form | powder to crystal |
| color | White to Almost white |
| Sensitive | Moisture Sensitive |
| BRN | 744474 |
| CAS DataBase Reference | 447-31-4(CAS DataBase Reference) |
| EPA Substance Registry System | Desyl chloride (447-31-4) |
Safety information for DESYL CHLORIDE
| Signal word | Danger |
| Pictogram(s) |
 Corrosion Corrosives GHS05  Exclamation Mark Irritant GHS07 |
| GHS Hazard Statements |
H314:Skin corrosion/irritation H335:Specific target organ toxicity, single exposure;Respiratory tract irritation |
| Precautionary Statement Codes |
P260:Do not breathe dust/fume/gas/mist/vapours/spray. P271:Use only outdoors or in a well-ventilated area. P280:Wear protective gloves/protective clothing/eye protection/face protection. P301+P330+P331:IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. P303+P361+P353:IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower. P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing. |
Computed Descriptors for DESYL CHLORIDE
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