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HomeProduct name listDESYL CHLORIDE

DESYL CHLORIDE

  • CAS NO.:447-31-4
  • Empirical Formula: C14H11ClO
  • Molecular Weight: 230.69
  • MDL number: MFCD00000858
  • EINECS: 207-181-7
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-07-29 17:07:33
DESYL CHLORIDE Structural

What is DESYL CHLORIDE?

Chemical properties

off-white to light beige powder

Purification Methods

For the purification of small quantities recrystallise it from pet ether (b 40-60o), but use MeOH or EtOH for larger quantities. For the latter solvent, dissolve 12.5g of chloride in 45mL of boiling EtOH (95%), filter and the filtrate yields colourless crystals (7.5g) on cooling. A further crop (0.9g) can be obtained by cooling in an ice-salt bath. It turns brown on exposure to sunlight but it is stable in sealed dark containers. The R(+)-enantiomer has m 75-76o (from pet ether) and []546.1 +168.4o (c 0.6, Me2CO) [Roger & Wood J Chem Soc 811 1954]. [Henley & Turner J Chem Soc 1182 1931, Ward Org Synth Coll Vol II 159 1943, Beilstein 7 H 436, 7 I 234, 7 II 369, 7 III 2106, 7 IV 1396.]

Properties of DESYL CHLORIDE

Melting point: 62-63 °C(lit.)
Boiling point: 330°C (rough estimate)
Density  1.1223 (rough estimate)
refractive index  1.5260 (estimate)
storage temp.  Store below +30°C.
form  powder to crystal
color  White to Almost white
Sensitive  Moisture Sensitive
BRN  744474
CAS DataBase Reference 447-31-4(CAS DataBase Reference)
EPA Substance Registry System Desyl chloride (447-31-4)

Safety information for DESYL CHLORIDE

Signal word Danger
Pictogram(s)
ghs
Corrosion
Corrosives
GHS05
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H314:Skin corrosion/irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P260:Do not breathe dust/fume/gas/mist/vapours/spray.
P271:Use only outdoors or in a well-ventilated area.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P301+P330+P331:IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P303+P361+P353:IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for DESYL CHLORIDE

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