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HomeProduct name listCYCLOPENTYL PHENYL KETONE

CYCLOPENTYL PHENYL KETONE

  • CAS NO.:5422-88-8
  • Empirical Formula: C12H14O
  • Molecular Weight: 174.24
  • MDL number: MFCD00001378
  • EINECS: 226-548-2
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-11-19 23:02:33
CYCLOPENTYL PHENYL KETONE Structural

What is CYCLOPENTYL PHENYL KETONE?

Description

Phenyl cyclopentyl ketone (Item No. 31036) is an analytical reference standard categorized as a precursor in the synthesis of ketamine (Item Nos. 19389 | 11630). This product is intended for research and forensic applications.

The Uses of CYCLOPENTYL PHENYL KETONE

Cyclopentyl Phenyl Ketone is used in the preparation of ortho-arylated compounds and phenanthrones by palladium-catalyzed chelation-assisted C-H activation of Cyclopentyl Phenyl Ketone.

The Uses of CYCLOPENTYL PHENYL KETONE

Phenylcyclopentyl ketone is the key intermediate of synthetic hydrochloric acid amyl ethyl quin ether.

Synthesis

In 100ml round-bottomed flask, by 2-cyclopenta ethyl benzoylacetate (10.6g, 43.05mmol, 1.0eq), NaOH (2.6g, 64.5mmol) and Na2CO3(4.5g, 43mmol), is suspended in 50.0mLH2In O, it is warmed up to 80 DEG C and reacts 3 hours, obtain product phenylcyclopentyl ketone.Purify: reactant liquor is cooled to room temperature, extract 3 times with ethyl acetate 20mL;Organic phase saturated sodium-chloride washs, and merges organic phase and uses anhydrous MgSO4Being dried, then remove solvent under reduced pressure, obtain thick product, column chromatography purifies, and eluant, eluent is ethyl acetate: petroleum ether (1:10), obtains 6.54g target product, yield 87.2%.

Properties of CYCLOPENTYL PHENYL KETONE

Boiling point: 136-140°C 16mm
Density  1,036 g/cm3
refractive index  1.5440
Flash point: >110°C
storage temp.  Sealed in dry,Room Temperature
solubility  Chloroform, Methanol (Slightly)
form  Oil
Specific Gravity 1.04
color  Pale Yellow
BRN  2045903
CAS DataBase Reference 5422-88-8(CAS DataBase Reference)
EPA Substance Registry System Methanone, cyclopentylphenyl- (5422-88-8)

Safety information for CYCLOPENTYL PHENYL KETONE

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H302:Acute toxicity,oral
H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
Precautionary Statement Codes P261:Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for CYCLOPENTYL PHENYL KETONE

InChIKey VYDIMQRLNMMJBW-UHFFFAOYSA-N

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