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HomeProduct name listEthyl 3-Amino-4-methylbenzoate

Ethyl 3-Amino-4-methylbenzoate

Ethyl 3-Amino-4-methylbenzoate Structural

What is Ethyl 3-Amino-4-methylbenzoate?

Synthesis

Dissolve 10 g of palladium on carbon (10%) and 140 g of ammonium formate in 400 ml of methanol, and then dissolve 136 g of ethyl 3-nitro-4-methylbenzoate (2) in 400 ml of methanol. Add the methanol solution of (2) dropwise to the reaction flask at room temperature. The reaction exotherms until the methanol boils. Continue the dropwise addition. After the dropwise addition, TLC detects the completion of the reaction and filters the palladium carbon. Concentrate the methanol, add 400ml of water, and filter to obtain 156g of white solid ethyl 3-amino-4-methylbenzoate (Ethyl 3-Amino-4-methylbenzoate) as a wet product, which can be used in the next step without drying.
Ethyl 3-Amino-4-methylbenzoate

Properties of Ethyl 3-Amino-4-methylbenzoate

Melting point: 48.6-50.1℃
Boiling point: 105°C/0.2mmHg(lit.)
Density  1.103±0.06 g/cm3(Predicted)
storage temp.  under inert gas (nitrogen or Argon) at 2–8 °C
solubility  soluble in Methanol
form  powder to crystal
pka 3.35±0.10(Predicted)
color  White to Almost white

Safety information for Ethyl 3-Amino-4-methylbenzoate

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
Precautionary Statement Codes P264:Wash hands thoroughly after handling.
P264:Wash skin thouroughly after handling.
P280:Wear protective gloves/protective clothing/eye protection/face protection.

Computed Descriptors for Ethyl 3-Amino-4-methylbenzoate

InChIKey MCNBNDUVWQEKNZ-UHFFFAOYSA-N

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