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HomeProduct name listAcid Orange 7

Acid Orange 7

Synonym(s):4-(2-Hydroxy-1-naphthylazo)benzenesulfonic acid sodium salt;Acid Orange 7;Acid Orange A;Orange II;Tropaeolin 000 No. 2

  • CAS NO.:633-96-5
  • Empirical Formula: C16H12N2O4S.Na
  • Molecular Weight: 351.33
  • MDL number: MFCD00011657
  • EINECS: 211-199-0
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2024-11-19 20:33:22
Acid Orange 7 Structural

What is Acid Orange 7?

Chemical properties

Orange-red powder

The Uses of Acid Orange 7

Acid Orange 7 (CAS# 633-96-5) is used as an azo dye pH indicator, it is an environmental pollutant.

Preparation

Acid Orange 7, commonly known as acidic orange II. 4-Aminobenzenesulfonic acid diazo, and Naphthalen-2-ol coupling. It is produced by azo coupling of β-naphthol and diazonium derivative of sulfanilic acid.

Definition

ChEBI: Acid orange 7 is a member of naphthalenes. Orange allergenic extract is used in allergenic testing.

Preparation

Acid orange 7 is produced by azo coupling of β-naphthol and diazonium derivative of sulfanilic acid.

Synthesis of Acid Orange 7

fig. Synthesis of Acid Orange 7

Flammability and Explosibility

Non flammable

Purification Methods

Purification is as for Orange I. Its solubility in H2O is 40g/L at 25o. [Müller et al. Helv Chim Acta 35 2579 1952.] Also purify it by extracting it with a small volume of cold water, then crystallising it by dissolving in boiling water, cooling to ca 80o, adding two volumes of EtOH and cooling. When cold, the precipitate is filtered off, washed with a little EtOH and dried in air. It can be salted out from aqueous solution with sodium acetate, then repeatedly extracted with EtOH. Meggy and Sims [J Chem Soc 2940 1956], after crystallising the sodium salt twice from water, dissolved it in cold water (11mL/g) and added conc HCl to precipitate the acid dye which was separated by centrifugation, redissolved and again precipitated with acid. After washing the precipitate three times with 0.5M acid, it was dried over NaOH, recrystallised twice from absolute EtOH, washed with a little Et2O, dried over NaOH and stored over conc H2SO4 in the dark. It can then be converted to the pure salt with the calculated amount of NaOH or Na2CO3. [Beilstein 16 IV 408.]

Properties and Applications

red light orange. Golden yellow powder. Soluble in water is red light yellow, orange soluble in alcohol. The strong sulfuric acid for quality in red, dilute create tan precipitation; In a golden of nitric acid; In the thick of sodium hydroxide solution not dissolve. Its water solution with hydrochloric acid generation tan precipitation; Add sodium hydroxide solution brown. In dyeing copper ions trend dark red in colour and lustre of iron ion shallow and dark. Discharge the gender is good. Mainly used for silk and wool dyeing, widely used in wool dyeing, can be used for wool, silk and polyamide fiber fabric of direct printing, leather and paper color, can also be used in indicator and biological shading. Is tasted can be used as a food dye, heavy metal salt used in organic pigments.

Standard Light Fastness Soaping Persperation Fastness Oxygen bleaching Fastness to seawater
Fading Stain Fading Stain Fading Stain
ISO 4 1 2 2-3 1 2 2 1
AATCC 5 1-2 1-2 1 1 1 3 3

Properties of Acid Orange 7

Melting point: 164°C
Density  1.525[at 20℃]
vapor pressure  0Pa at 25℃
storage temp.  Amber Vial, -20°C Freezer, Under inert atmosphere
solubility  Solubility Very soluble in water; very slightly soluble in ethanol
Colour Index  15510
form  Crystalline Powder
pka 8.26, 11.4(at 25℃)
color  Green to blue
Odor Odorless
PH Range Amber (7.4) to orange (8.6);Orange (10.2) to red (11.8)
Water Solubility  116 g/L (30 ºC)
λmax 483nm
Merck  14,6858
BRN  3898201
Stability: Light Sensitive
Biological Applications Cosmetics; wound dressing materials
Major Application Organic light emitting diodes (OLEDs), nanoparticles, inks, wood preservatives, textiles, hair dyes, cosmetics, wound dressing materials, biofuel cells
CAS DataBase Reference 633-96-5(CAS DataBase Reference)
EPA Substance Registry System C.I. Acid Orange 7, monosodium salt (633-96-5)

Safety information for Acid Orange 7

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
Precautionary Statement Codes P264:Wash hands thoroughly after handling.
P264:Wash skin thouroughly after handling.
P280:Wear protective gloves/protective clothing/eye protection/face protection.

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