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HomeProduct name list6-Methoxyisoquinoline

6-Methoxyisoquinoline

6-Methoxyisoquinoline Structural

What is 6-Methoxyisoquinoline?

Chemical properties

Clear Oil

The Uses of 6-Methoxyisoquinoline

6-Methoxy Isoquinoline (cas# 52986-70-6) is a compound useful in organic synthesis.

Preparation

6-Methoxyisoquinoline synthesis: Using benzaldehyde as the starting material, m-methoxybenzaldehyde is obtained through nitration, reduction, diazotization, hydrolysis and methylation, and 3-methoxybenzaldehyde is obtained through condensation with nitromethane Shiff base and reduction of aluminum hydride -p-Phenylethylamine. The Pictet-Spengler reaction of 3-methoxyl-p-phenylethylamine and 40% aqueous formaldehyde produces 6-methoxyl-1,2,3,4-tetrahydroisoquinoline, and then obtains the target compound in dehydrogenation 6-Methoxyisoquinoline.

Synthesis Reference(s)

Journal of the American Chemical Society, 69, p. 1939, 1947 DOI: 10.1021/ja01200a028

Properties of 6-Methoxyisoquinoline

Boiling point: 88-95?C/0.8 Torr
Density  1.130±0.06 g/cm3(Predicted)
storage temp.  Sealed in dry,Room Temperature
solubility  Chloroform, Dichloromethane
form  Oil
pka 6.11±0.10(Predicted)
color  Pale Yellow
CAS DataBase Reference 52986-70-6(CAS DataBase Reference)

Safety information for 6-Methoxyisoquinoline

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P261:Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for 6-Methoxyisoquinoline

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