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HomeProduct name list4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane

4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane

4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane Structural

What is 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane?

The Uses of 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane

4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly for laboratory research and development Process and chemical production process.

Synthesis

Synthesis_890042-13-4
In a nitrogen atmosphere, 100 g (326 mmol) of 2-bromotriphenylene was dissolved in dimethylformamide(Pinacolato diboron) 99.2 (manufactured by Wako Pure Chemical Industries, Ltd.) was dissolved in 1,000 mL of dimethylformamide (DMF)G (391 mmol) and 1,1'-bis (diphenylphosphine) ferrocene) dichloropalladium (II) (1,1-Bis (diphenylphosphine) ferrocene) dichloropalladium (II)) 2.66 g (3.26 mmol) and potassium acetate 80 g (815 mmol) of potassium acetate were added and the mixture was refluxed by heating at 150 DEG C for 5 hours. After completing the reaction,Water was added to the solution, the mixture was filtered, and then dried in a vacuum oven. The thus obtained residue was purified by flash column chromatographyTo obtain 113 g (98%) of the compound I-1. HRMS (70 eV, EI +): m / z Calcd for C24H23BO2: 354.1791, found

Properties of 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane

Melting point: 174.0 to 178.0 °C
Boiling point: 544.9±19.0 °C(Predicted)
Density  1.16±0.1 g/cm3(Predicted)
storage temp.  Sealed in dry,Room Temperature
form  powder to crystal
color  White to Orange to Green

Safety information for 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H302:Acute toxicity,oral
H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
H335:Specific target organ toxicity, single exposure;Respiratory tract irritation
Precautionary Statement Codes P261:Avoid breathing dust/fume/gas/mist/vapours/spray.
P280:Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312:IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352:IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for 4,4,5,5-TetraMethyl-2-(3-triphenylen-2-yl-phenyl)-[1,3,2]dioxaborolane

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