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HomeProduct name list2,6-Pyridinedicarboxylic acid monomethyl ester

2,6-Pyridinedicarboxylic acid monomethyl ester

  • CAS NO.:7170-36-7
  • Empirical Formula: C8H7NO4
  • Molecular Weight: 181.15
  • MDL number: MFCD00806109
  • EINECS: 808-166-3
  • SAFETY DATA SHEET (SDS)
  • Update Date: 2023-06-08 17:06:38
2,6-Pyridinedicarboxylic acid monomethyl ester  Structural

What is 2,6-Pyridinedicarboxylic acid monomethyl ester ?

Physical properties

White or off white powder
    

The Uses of 2,6-Pyridinedicarboxylic acid monomethyl ester

2,6-Pyridinedicarboxylic Acid Monomethyl Ester can be used as chemical scavengers.

Synthesis Reference(s)

Synthetic Communications, 25, p. 739, 1995 DOI: 10.1080/00397919508011411

Synthesis

To a solution of Dimethyl 2,6-pyridinedicarboxylate (10.0 g, 51.2 mmol) in MeOH (300 mL) was added KOH (2.89 g, 51.2 mmol) and themixture was stirred overnight at rt. After the removal of the solvent, the residue was diluted with water. Theaqueous layer was washed with AcOEt and acidified with conc. HCl aq, and then the mixture was extracted withthe solution of CHCl3/isopropanol (3/1 (v/v)). The organic layer were dried over MgSO4 and concentrated invacuo to give 2,6-Pyridinedicarboxylic acid monomethyl ester (8.17 g, 87 percent) as a white solid.

Properties of 2,6-Pyridinedicarboxylic acid monomethyl ester

Melting point: 144-146°C
Boiling point: 393°C
Density  1.361±0.06 g/cm3(Predicted)
storage temp.  Keep in dark place,Sealed in dry,Room Temperature
solubility  soluble in Methanol
form  powder to crystal
pka 3.27±0.10(Predicted)
color  White to Almost white
InChI InChI=1S/C8H7NO4/c1-13-8(12)6-4-2-3-5(9-6)7(10)11/h2-4H,1H3,(H,10,11)
CAS DataBase Reference 7170-36-7(CAS DataBase Reference)

Safety information for 2,6-Pyridinedicarboxylic acid monomethyl ester

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H315:Skin corrosion/irritation
H319:Serious eye damage/eye irritation
Precautionary Statement Codes P280:Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352:IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313:IF SKIN irritation occurs: Get medical advice/attention.
P337+P313:IF eye irritation persists: Get medical advice/attention.

Computed Descriptors for 2,6-Pyridinedicarboxylic acid monomethyl ester

InChIKey VWIOMFMPIVMLIR-UHFFFAOYSA-N
SMILES C1(C(OC)=O)=NC(C(O)=O)=CC=C1

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