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HomeProduct name list1-bromodibenzo[b,d]furan

1-bromodibenzo[b,d]furan

1-bromodibenzo[b,d]furan Structural

What is 1-bromodibenzo[b,d]furan?

The Uses of 1-bromodibenzo[b,d]furan

1-bromodibenzo[b,d]furan can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development and chemical and pharmaceutical production processes.

Synthesis

Synthesis_50548-45-3
111 g (416 mmol) of 6?ˉ-bromo-2?ˉ-fluorobiphenyl-2-ol are dissolved in 21 of SeccoSolv DMF (max 0.003% of H20) and cooled to 5??C. 20 g (449 mmol) of sodium hydride (60% suspension in paraffin oil) are added in portions tothis solution, and the mixture is stirred for a further 20 mm. after the addition is complete and then heated at 100??C for 45 mm. After cooling, 500 ml of ethanol are slowly added to the mixture, which is then evaporated to dryness in a rotary evaporator and purified by chromatography. Yield: 90 g (367 mmol), 88.5% of theory.

Properties of 1-bromodibenzo[b,d]furan

Melting point: 67℃
Boiling point: 343.8±15.0 °C(Predicted)
Density  1.577±0.06 g/cm3(Predicted)
storage temp.  Sealed in dry,Room Temperature
form  powder to crystal
color  White to Gray to Brown

Safety information for 1-bromodibenzo[b,d]furan

Signal word Warning
Pictogram(s)
ghs
Exclamation Mark
Irritant
GHS07
GHS Hazard Statements H302:Acute toxicity,oral
Precautionary Statement Codes P280:Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338:IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Computed Descriptors for 1-bromodibenzo[b,d]furan

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