2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
| Price | USD1.00 | USD2.00 |
| Packge | 1KG | 1KG |
- Min. Order:1KG
- Supply Ability:200kg
- Time:2019-09-02
Product Details
- Product Name2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
- CAS No.58632-95-4
- EINECS No.261-370-9
- MFC13H14N2O3
- MW246.26
- InChIKeyQQWYQAQQADNEIC-UHFFFAOYSA-N
- AppearanceFine Crystalline PowderWhite to slightly beige
- storage temp. -20°C
- Water Solubility insoluble
- Melting point 85-88 °C (lit.)
- Boiling point 389.26°C (rough estimate)
- density 1.1855 (rough estimate)
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Product Name:
Synonyms:
alpha-[[[(1,1-dimethylethoxy)carbonyl]oxy]imino]-benzeneacetonitril;N-TERT-BUTOXYCARBONYLOXYIMINO-2-PHENYLACETONITRILE;2-(tert-Butoxycarbon;Boc-ON 2-(tert-ButoxycarbonyloxyiMino)-2-phenylacetonitrile;BOC-ON, 99% 25GR;BOC-ON, 99% 5GR;LABOTEST-BB LT00159655;BOC-ON
CAS:
MF:
C13H14N2O3
MW:
246.26
EINECS:
261-370-9
Product Categories:
Mol File:
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2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile Chemical Properties
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Melting point
85-88 °C(lit.)
Boiling point
389.26°C (rough estimate)
density
1.1855 (rough estimate)
refractive index
1.6450 (estimate)
storage temp.
2-8°C
form
Fine Crystalline Powder
color
White to slightly beige
Water Solubility
insoluble
Sensitive
Moisture Sensitive
BRN
2217296
CAS DataBase Reference
EPA Substance Registry System
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Safety Information
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Hazard Codes
Risk Statements
Safety Statements
RIDADR
3276
WGK Germany
3
RTECS
DA0513600
F
TSCA
Yes
HazardClass
6.1
PackingGroup
III
HS Code
29280090
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English
English
English
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2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile Usage And Synthesis
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Chemical Properties
White to off-white microcrystalline powder
Purification Methods
Triturate the solid with 90% aqueous MeOH, filter, wash with 90% aqueous MeOH and dry it in a vacuum. Recrystallise it from MeOH (needles or plates), but use warm MeOH and cool to crystallise; do not boil as it decomposes slowly. IR has max 1785 (C=O) cm-1 and NMR (CDCl3) usually shows two tert-butyl singlets for syn and anti isomers. Store it in a brown bottle (fridge). It evolves CO2 at room temperature (stoppered bottle can explode!), but can be stored over silica gel which may extend its useful life to more than a year. [Itoh et al. Org Synth 59 95 1980.]
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2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile Preparation Products And Raw materials
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Preparation Products
Company Profile Introduction
Henan CoreyChem Co., Ltd, based on the original Zhengzhou Cote Chemical Research Institute, be brave in absorbing highly educated talents & overseas returnees; actively responded to Zhengzhou City High-tech Zone Government’s Special Care Policy, reorganized and founded in National University of Science and Technology Park, which is a high-tech, stock enterprise of high-end chemical Custom synthesis;The park was created by the People's Government of Henan Province, and proved by Ministry of Education and the National Science & Technology, taking the construction mode of "many college a park, and common development", mainly depends on Zhengzhou University and Henan University’s scientific research and talent advantage to set up Universities, scientific research institute and enterprise scientific research achievements transformation platform, to make high-tech enterprises incubate, is the new high-tech talent gathering base, high and new technology industry enterprise radiation base, colleges and universities technological innovation base.
Henan Coreychem Co., Ltd, facing global High-tech pharmaceutical raw materials, high complex new type intermediates, fine chemicals custom synthesis, scale-up production and Rare chemicals trade. Corey have well-equipped machine, strong technical force and considerate marketing team service. We also have rich experience advantage in basic research, small scale process development, scale-up, industrial technology development & production and cost control.
Recommended supplier
- Since:2014-12-17
- Address: No.967,15th Floor,Unit 7, Building 1, No.70 of DianChang Road, High-tech Development Zone, Zhengzho
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